A new method for the synthesis of fluorinated vinyl sulfides and ketene dithioacetals

被引：5
|
作者：
Kovregin, AN [1 ]
Sizov, AY [1 ]
Ermolov, AF [1 ]
机构：
[1] Mil Univ Radiat Chem & Biol Def, Moscow 107005, Russia
来源：
RUSSIAN CHEMICAL BULLETIN | 2001年 / 50卷 / 06期
关键词：
CH-acids; thiols; fluorinated vinyl sulfides; fluorinated ketene dithioacetals; dehydrofluorination; BF(3)center dot NEt(3);
D O I：
10.1023/A:1011325520421
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new method was developed for the synthesis of fluorine-containing functionally substituted vinyl sulfides and ketene dithioacetals from the corresponding derivatives of a-trifluoromethyl-substituted CH-acids and thiols in the presence of BF(3) . NEt(3).
引用
下载
收藏
页码：1044 / 1046
页数：3
相关论文
共 50 条
  • [1] A new method for the synthesis of fluorinated vinyl sulfides and ketene dithioacetals
    A. N. Kovregin
    A. Yu. Sizov
    A. F. Ermolov
    Russian Chemical Bulletin, 2001, 50 : 1044 - 1046
  • [2] A new method for the synthesis α-acetyll ketene dithioacetals
    Zhao, YL
    Liu, Q
    Zhang, W
    Yu, HF
    Liu, Y
    Lin, C
    CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 2006, 27 (03): : 482 - 484
  • [3] A new method for the synthesis of alpha-aroyl ketene dithioacetals
    Fang, QX
    Liu, Q
    Hu, YL
    Lin, C
    CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE, 1995, 16 (12): : 1896 - 1898
  • [4] SYNTHESIS OF FLUORINATED VINYL SULFIDES AND SELENIDES
    PIETTRE, S
    DECOCK, C
    MERENYI, R
    VIEHE, HG
    TETRAHEDRON, 1987, 43 (19) : 4309 - 4319
  • [5] Ketene dithioacetals in organic synthesis
    Huang, Lifeng
    Wu, Jinjing
    Hu, Jingang
    Bi, Yicheng
    Huang, Dayun
    TETRAHEDRON LETTERS, 2020, 61 (04)
  • [6] Synthesis of dithioacetals via gold-catalysed hydrothiolation of vinyl sulfides
    Murugesh, Venkatesh
    Ryou, Bokyeong
    Park, Cheol-Min
    ORGANIC & BIOMOLECULAR CHEMISTRY, 2023, 21 (03) : 585 - 589
  • [7] SYNTHESIS OF HETEROAROMATIC KETENE DITHIOACETALS
    GOODWIN, JA
    KWOK, IMY
    WAKEFIELD, BJ
    SYNTHESIS-STUTTGART, 1990, (11): : 991 - 992
  • [8] Fluorinated ketene dithioacetals.: Part 7:: New β-halo perfluorodithiocrotonic acid esters from perfluoroketene dithioacetals
    Bouillon, JP
    Shermolovich, YG
    Portella, C
    TETRAHEDRON LETTERS, 2001, 42 (11) : 2133 - 2135
  • [9] Iododecarboxylation reactions of α-oxo ketene dithioacetals:: The new route to α-iodo ketene dithioacetals
    Zhao, YL
    Liu, Q
    Sun, R
    Zhang, Q
    Xu, XX
    SYNTHETIC COMMUNICATIONS, 2004, 34 (03) : 463 - 469
  • [10] FLUORINATED KETENE DITHIOACETALS .2. SYNTHESIS OF 2-HYDROPERFLUORO ACID-DERIVATIVES FROM PERFLUOROKETENE DITHIOACETALS
    MUZARD, M
    PORTELLA, C
    JOURNAL OF ORGANIC CHEMISTRY, 1993, 58 (01): : 29 - 31
12345