Synthesis of [3H]-higenamine

被引：1
|
作者：
Wu, DZ
Zhang, Z
Chen, BL
Lil, GF
机构：
[1] China Inst Atom Energy, Beijing 102413, Peoples R China
[2] Chinese Acad Med Sci, Cardiovasc Inst, Beijing 100037, Peoples R China
[3] Chinese Acad Med Sci, Fu Wai Hosp, Beijing 100037, Peoples R China
[4] Peking Union Med Coll, Beijing 100037, Peoples R China
来源：
JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2003年 / 258卷 / 03期
关键词：
D O I：
10.1023/B:JRNC.0000011772.32047.e5
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The synthesis of [H-3]-higenamine by a four steps reaction, namely condensation, cyclization, catalytic tritiation and demethoxylation is described. The acidulated product was purified by thin layer chromatography and the final component has a high specific activity and radiochemical purity.
引用
收藏
页码：689 / 691
页数：3
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