Synthesis and crystal structure of 1,7-(NH3)2B12H10 • 0.5H2O

被引：0
|
作者：
Dudenkov, IV [1 ]
Zhizhin, KY [1 ]
Chernyavskii, AS [1 ]
Katser, SB [1 ]
Goeva, LV [1 ]
Sergienko, VS [1 ]
Solntsev, KA [1 ]
Kuznetsov, NT [1 ]
机构：
[1] Russian Acad Sci, NS Kurnakov Gen & Inorgan Chem Inst, Moscow 117907, Russia
来源：
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2000年 / 45卷 / 12期
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D O I：
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中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
1,7-Diaminoundecahydro-closo-dodecaborate was synthesized and characterized. Crystals are orthorhombic, space group Pna2(1), a = 22.99(1) Angstrom, b = 10.293(6) Angstrom, c = 9.323(6) Angstrom, V = 2206(2) Angstrom (3), Z = 8. Crystals contain two independent identical neutral molecules 1,7-(NH3)(2)B12H10 and one water molecule of crystallization. The arrangement of the NH3 substituents corresponds to the meta isomer.
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页码：1864 / 1867
页数：4
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