The crystal structure of dichlorobis(2-(dicyclohexylphosphino)-2′,4′,6′-tri-i-propyl-1,1′-biphenyl) palladium(II)-dichloroform, C68H100Cl8P2Pd

被引：0
|
作者：
Liu, Hui [1 ]
机构：
[1] Zhengzhou Normal Univ, Sch Chem & Chem Engn, Zhengzhou 450044, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2020年 / 235卷 / 03期
关键词：
SUZUKI; PRECATALYSTS; COMPLEXES; CATALYSTS; SCOPE;
D O I：
10.1515/ncrs-2020-0012
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C68H100Cl8P2Pd, triclinic, P (1 ) over bar (no. 2), a = 9.6961(4) angstrom, b =13.6069(6) angstrom, c = 15.1642(5) angstrom, alpha = 88.456(3)degrees, beta = 72.251(3)degrees, gamma = 72.376(4)degrees, V =1811.64(12) angstrom(3), Z =1, R-gt(F) = 0.0483, wR(ref)(F-2) = 0.1332, T =291 K.
引用
收藏
页码：755 / 757
页数：3
相关论文
共 50 条
  • [31] Interaction of cystamine with palladium(II) monoethanolaminate complex:: Crystal structure of [Pd(NH2CH2CH2OH)4][Pd6(NH2CH2CH2S)8]Cl6 • 5H2O
    Gasanov, KI
    Antsyshkina, AS
    Sadikov, GG
    Ivanova, NA
    Mirzai, DI
    Efimenko, IA
    Sergienko, VS
    CRYSTALLOGRAPHY REPORTS, 2002, 47 (04) : 603 - 609
  • [32] Interaction of cystamine with palladium(II) monoethanolaminate complex: Crystal structure of [Pd(NH2CH2CH2OH)4][Pd6(NH2CH2CH2S)8]Cl6 · 5H2O
    Kh. I. Gasanov
    A. S. Antsyshkina
    G. G. Sadikov
    N. A. Ivanova
    D. I. Mirzai
    I. A. Efimenko
    V. S. Sergienko
    Crystallography Reports, 2002, 47 : 603 - 609
  • [33] Novel structures of cyclometallated complexes of palladium(II) derived from terdentate ligands.: Crystal and molecular structure of [Pd{C6H4C(H)=NCH2CH2CH2NMe2}(X)] (X = Cl, Br, I)
    Fernández, A
    Uría, P
    Fernández, JJ
    López-Torres, M
    Suárez, A
    Vázquez-García, D
    Pereira, T
    Vila, JM
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2001, 620 (1-2) : 8 - 19
  • [34] Polynuclear cyclometallated palladium(II) complexes.: Crystal and molecular structures of [(PPh3)(Cl)PdN(Cy)=C(H)C6H2C(H)=N(Cy) Pd(Cl)(PPh3)] and [{PdN(Cy)=C(H)C6H2C(H)=N(Cy)Pd}{Ph2PC(H)=C(H)PPh2-P,P}2][ClO4]2
    López-Torres, M
    Fernández, A
    Fernández, JJ
    Suárez, A
    Castro-Juiz, S
    Pereira, MT
    Vila, JM
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2002, 655 (1-2) : 127 - 133
  • [35] Crystal structure of tetraaquatetrakis(1,10-phenanthroline)bis(μ-1,1′-biphenyl-2,2′-dicarboxylato)dilanthanum(III) dichloride tetrahydrate, [La2(H2O)4(C12H8N2)4(C14H8O4)2]Cl2 .4H2O
    Hu, ML
    Miao, Q
    Shi, Q
    Cheng, YQ
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2004, 219 (04): : 442 - 444
  • [36] Crystal structure of tetra[(2,6-dicarboxylato-2′,6′-dicarboxy-1,1′-biphenyl)-(6,6′-dimethyl-2,2′-bipyridine)copper(II)] pentahydrate, [Cu(C16H8O8)(C12H12N2)]4 • 5H2O
    Hu, Xi-Ying
    Wang, Jian-Xu
    Shan, Wen-Wen
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2012, 227 (02): : 227 - 229
  • [37] Crystal structure of trans-diiodidobis(4-phenylpyridine-κN)palladium(II), C22H18I2N2Pd
    Ha, Kwang
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2013, 228 (02): : 257 - 258
  • [38] Crystal structure of (2,2′-bipyrimidine-κ2N,N′) dibromidopalladium(II), C8H6Br2N4Pd
    Ha, Kwang
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2014, 229 (02): : 149 - 150
  • [39] Synthesis and characterization of pyrrolthiosemicarbazone complexes of palladium(II).: Crystal structures of [{Pd[C4H4NC(H)=NNC(S)NHMe](Cl)}2{μ-Ph2P(CH2)3PPh2}] and [Pd{C4H4NC(H)=NNC(S)NHMe}{Ph2P(CH2)2PPh2-P,P}](Cl)
    Adrio, L
    Alberdi, G
    Amoedo, A
    Lata, D
    Fernández, A
    Martínez, J
    Pereira, MT
    Vila, JM
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2005, 631 (11): : 2197 - 2203
  • [40] CRYSTAL-STRUCTURE AND MOLECULAR-STRUCTURE OF CIS-BIS[DICYCLOHEXYLPHOSPHINO-N-PHENYL(THIOFORMAMIDO)]PALLADIUM(II) - CIS-[PD((C-C6H11)(2)PC(S)=N(C6H5))(2)]
    KLEIN, W
    KRAMOLOWSKY, R
    SIASIOS, G
    TIEKINK, ERT
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 1995, 210 (05): : 348 - 351
12345