Synthesis and characterization of quaternized poly(phthalazinone ether sulfone ketone) for anion-exchange membrane

被引：37
|
作者：
Ran, Xi Gao [1 ]
Yan, Chun
Zhang, Hua Min
Zhang, Shou Hai
Liu, Cheng
Zhao, Ping
机构：
[1] Dalian Univ Technol, Dept Polymer Mat, Dalian 116012, Peoples R China
[2] Chinese Acad Sci, Dalian Inst Chem Phys, PEMFC Key Mat & Technol Lab, Dalian 116023, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2007年 / 18卷 / 10期
基金：
中国国家自然科学基金;
关键词：
chloromethylation; quaternization; poly(phthalazinone ether sulfone ketone); anion-exchange membrane; vanadium redox flow battery;
D O I：
10.1016/j.cclet.2007.08.022
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Chloromethylated poly(phthalazinone ether sulfone ketone) (CMPPESK) was prepared from poly(phthalazinone ether sulfone ketone) (PPESK) using chloromethyl octyl ethers (CMOE) with lower toxicity as chloromethylated regent. CMPPESK was soluble in N-methyl-2-pyrrolidone (NMP), N,N-dimethylacetamide (DMAc) and chloroform. Quaternized poly(phthalazinone ether sulfone ketone) (QAPPESK) was prepared from CMPPESK by quaternization. QAPPESK had excellent solvent resistance, which was only partly soluble in sulfuric acid (98%) and swollen in N,N-dimethylformamide (DMF). The vanadium redox. flow battery (V-RFB) using QAPPESK anion-exchange membrane had better performance with 88.3% of overall energy efficiency. (c) 2007 Published by Elsevier B.V. on behalf of Chinese Chemical Society.
引用
收藏
页码：1269 / 1272
页数：4
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