Determination of Phenol in the Bangsai River Water of Bangladesh by Gas Chromatography-Mass Spectrometry

被引:2
|
作者
Hossain, M. Amzad [1 ]
Yeasmin, Farida
Rahman, S. M. Mizanur
Rana, M. S.
Fatema, Konica J.
机构
[1] Atom Energy Ctr, Div Chem, Dhaka, Bangladesh
关键词
Environmental organic pollutants; toxic phenolic compounds; liquid-phase extraction; preconcentration; GC-MS; LIQUID-CHROMATOGRAPHY; ULTRAVIOLET;
D O I
10.3103/S1063455X11020044
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
A simple, sensitive and rapid gas chromatography-mass spectrometry (GC-MS) method is proposed for the analysis of some environmentally important highly toxic phenols in water. The concentration level of phenol was determined in water at the sampling stations of Savar, Dhaka Export Processing Zone (DEPZ) and Bank Colony of the Bangsai River, Bangladesh. Water samples were collected from different depth of the sampling stations. The phenolic compounds were extracted with dichloromethane, which was further preconcentrated by evaporation. Different concentrations of toxic phenol were obtained in the river water at the various sampling stations. The concentration of highly toxic phenol was found in the range of 0.01-0.998 mu g L(-1). This method could permit the analysis of water for phenol as well as phenolic derivatives with detection limit as low as 100 ng L(-1).
引用
收藏
页码:91 / 96
页数:6
相关论文
共 50 条
  • [31] Determination of dimethyldicarbonate in wine by gas chromatography-mass spectrometry
    Chen, Bo
    Luo, Jie
    Wan, Zhigang
    Yi, Bingqing
    Tu, Xiaoke
    He, Chundian
    Jin, Baohui
    [J]. Chinese Journal of Analysis Laboratory, 2023, 42 (12) : 1678 - 1682
  • [32] Determination of Levamisole in Urine by Gas Chromatography-Mass Spectrometry
    Trehy, Michael L.
    Brown, Daniel J.
    Woodruff, Jeffrey T.
    Westenberger, Benjamin J.
    Nychis, William G.
    Reuter, Nicholas
    Schier, Joshua G.
    Vagi, Sara J.
    Hwang, Rong-Jen
    [J]. JOURNAL OF ANALYTICAL TOXICOLOGY, 2011, 35 (08) : 545 - 550
  • [33] Determination of Pesticides in Carrots by Gas Chromatography-Mass Spectrometry
    Covaciu, Florina D.
    Magdas, D. Alina
    Marincas, Olivian
    Moldovan, Zaharie
    [J]. ANALYTICAL LETTERS, 2017, 50 (17) : 2665 - 2676
  • [34] Sensitive determination of glutaraldehyde in environmental water by derivatization and gas chromatography-mass spectrometry
    Kang, Hye-In
    Shin, Ho-Sang
    [J]. ANALYTICAL METHODS, 2016, 8 (15) : 3216 - 3223
  • [35] Determination of Acetochlor Residue in Food by Gas Chromatography and Gas Chromatography-Mass Spectrometry
    Dong Zhen-Lin
    Yang Chun-Guang
    Xiao Shan-Shan
    Zhao Jing-Hong
    Li Yi-Chen
    [J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2009, 37 (05) : 698 - 702
  • [36] Degradation of bisphenol A by ozonation and determination of degradation intermediates by gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry
    Kusvuran, Erdal
    Yildirim, Deniz
    [J]. CHEMICAL ENGINEERING JOURNAL, 2013, 220 : 6 - 14
  • [37] Fully automated liquid chromatography-mass spectrometry determination of 17β-estradiol in river water
    Watabe, Yoshiyuki
    Kubo, Takuya
    Nishikawa, Teppei
    Fujita, Tomio
    Kaya, Kunimitsu
    Hosoya, Ken
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2006, 1120 (1-2) : 252 - 259
  • [38] Determination of polybrominated diphenyl ethers in river water by combination of liquid-liquid extraction and gas chromatography-mass spectrometry
    Zhang, Weifei
    Lin, Xuexia
    Li, Hai-Fang
    Wang, Zhihua
    Lin, Jin-Ming
    [J]. CHINESE CHEMICAL LETTERS, 2014, 25 (09) : 1225 - 1229
  • [39] Simultaneous determination of non-steroidal anti-inflammatory drugs in river water by gas chromatography-mass spectrometry
    Shin, Ho-Sang
    Oh, Jin-Aa
    [J]. JOURNAL OF SEPARATION SCIENCE, 2012, 35 (04) : 541 - 547
  • [40] Cellulose membrane modified with polypyrrole as an extraction device for the determination of emerging contaminants in river water with gas chromatography-mass spectrometry
    de Noronha, Barbara Viero
    Bergamini, Marcio Fernando
    Marcolino Junior, Luiz Humberto
    Goncalves da Silva, Bruno Jose
    [J]. JOURNAL OF SEPARATION SCIENCE, 2018, 41 (13) : 2790 - 2798