Synthesis and characterization of barium molybdate nanostructures with the aid of amino acids and investigation of its photocatalytic degradation of methyl orange

被引:16
|
作者
Gholami, Ali [1 ]
Maddahfar, Mahnaz [2 ]
机构
[1] Univ Kashan, Dept Analyt Chem, Fac Chem, Kashan, Iran
[2] Islamic Azad Univ, Arak Branch, Young Researchers & Elites Club, Arak, Iran
关键词
MICROWAVE-ASSISTED SYNTHESIS; HYDROTHERMAL SYNTHESIS; OPTICAL-PROPERTIES; FACILE SYNTHESIS; PHOTOLUMINESCENCE; POWDERS; NANOPARTICLES; GROWTH; ROUTE; BAWO4;
D O I
10.1007/s10854-016-4627-x
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
In the current study, barium molybdate (BaMoO4) nanostructures were synthesized via a large-scale and facile sonochemical method based on the reaction between barium(II) nitrate hexahydrate and (NH4)(6)Mo7O24 center dot 4H(2)O in an aqueous solution. Besides, two amino acids leucine and proline were introduce as capping agents and their effects on the morphology and particle size of barium molybdate were investigated. It was found that size and morphology could be easily realized by changing the type of amino acids. XRD, SEM, EDS, and UV-Vis spectroscopy were employed to characterize structural, morphological, and optical properties of BaMoO4 nanostructures. Barium molybdate (BaMoO4) nanostructures indicated a ferromagnetic behavior at room temperature, as evidenced by using vibrating sample magnetometer. Furthermore, the photocatalysis results reveal that the maximum decolorization of 75 % for methyl orange occurred with BaMoO4 samples in 70 min under ultraviolet light irradiation.
引用
收藏
页码:6773 / 6778
页数:6
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