The influence of synthesis conditions on the surface state of detonation nanodiamonds

被引：2
|
作者：
Panova, A. N. [1 ]
Dolmatov, V. Yu. [2 ]
Ishchenko, E. V. [3 ]
Tsapyuk, G. G. [3 ]
Bochechka, A. A. [1 ]
Veretennikova, M. V. [2 ]
Myllymaki, V. [4 ]
Nikitin, E. V. [5 ]
机构：
[1] Natl Acad Sci Ukraine, Bakul Inst Superhard Mat, UA-04074 Kiev, Ukraine
[2] Tekhnolog Fed State Unitary Enterprise, Special Design Technol Bur FSUE SDTB, St Petersburg 192076, Russia
[3] Taras Shevchenko Natl Univ Kiev, UA-01601 Kiev, Ukraine
[4] Carbodeon Ltd Oy, T Vantaa, Finland
[5] OOO SIDAL, Lesnoi, Russia
来源：
JOURNAL OF SUPERHARD MATERIALS | 2015年 / 37卷 / 03期
关键词：
detonation nanodiamonds; thermal desorption; doping; surface modification; detonation synthesis; crystal lattice; functional groups;
D O I：
10.3103/S1063457615030089
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The paper addresses thermal desorption of volatile products from the surface of detonation nanodiamonds modified in the process of synthesis. Their possible doping is shown to have a slight effect on the behavior and temperature range of evolution of atomic oxygen, water, carbon monoxide and dioxide. The atomic oxygen spectrum has two peaks (at 250-300 and 550-650A degrees C), emission of water has three peaks (at 50-80, 220-260, and 550-600A degrees C), the evolution of CO has a single peak at 600-760A degrees C, and that of CO2 has two peaks (at 200-270 and 520-660A degrees C). Phosphorus-containing detonation nanodiamonds have been found to evolve phosphine over the entire temperature range of nanodiamond treatment.
引用
收藏
页码：202 / 210
页数：9
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