The influence of synthesis conditions on the surface state of detonation nanodiamonds

被引：2

作者：

Panova, A. N. ^{[1
]}

Dolmatov, V. Yu. ^{[2
]}

Ishchenko, E. V. ^{[3
]}

Tsapyuk, G. G. ^{[3
]}

Bochechka, A. A. ^{[1
]}

Veretennikova, M. V. ^{[2
]}

Myllymaki, V. ^{[4
]}

Nikitin, E. V. ^{[5
]}

机构：

[1] Natl Acad Sci Ukraine, Bakul Inst Superhard Mat, UA-04074 Kiev, Ukraine

[2] Tekhnolog Fed State Unitary Enterprise, Special Design Technol Bur FSUE SDTB, St Petersburg 192076, Russia

[3] Taras Shevchenko Natl Univ Kiev, UA-01601 Kiev, Ukraine

[4] Carbodeon Ltd Oy, T Vantaa, Finland

[5] OOO SIDAL, Lesnoi, Russia

来源：

JOURNAL OF SUPERHARD MATERIALS | 2015年 / 37卷 / 03期

关键词：

detonation nanodiamonds; thermal desorption; doping; surface modification; detonation synthesis; crystal lattice; functional groups;

D O I：

10.3103/S1063457615030089

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

The paper addresses thermal desorption of volatile products from the surface of detonation nanodiamonds modified in the process of synthesis. Their possible doping is shown to have a slight effect on the behavior and temperature range of evolution of atomic oxygen, water, carbon monoxide and dioxide. The atomic oxygen spectrum has two peaks (at 250-300 and 550-650A degrees C), emission of water has three peaks (at 50-80, 220-260, and 550-600A degrees C), the evolution of CO has a single peak at 600-760A degrees C, and that of CO2 has two peaks (at 200-270 and 520-660A degrees C). Phosphorus-containing detonation nanodiamonds have been found to evolve phosphine over the entire temperature range of nanodiamond treatment.

引用

页码：202 / 210

页数：9

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[1] The influence of synthesis conditions on the surface state of detonation nanodiamonds
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V. Yu. Dolmatov
E. V. Ishchenko
G. G. Tsapyuk
A. A. Bochechka
M. V. Veretennikova
V. Myllymaki
E. V. Nikitin
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