Solid-state synthesis of "bamboo-like" and straight carbon nanotubes by thermolysis of hexa-peri-hexabenzocoronene-cobalt complexes

被引:57
|
作者
Wu, JS
El Hamaoui, B
Li, JX
Zhi, LJ
Kolb, U
Müllen, K
机构
[1] Max Planck Inst Polymer Res, D-55128 Mainz, Germany
[2] Univ Mainz, Inst Phys Chem, D-55128 Mainz, Germany
关键词
carbon nanotubes; cobalt; electron microscopy; precursor synthesis; thermolysis;
D O I
10.1002/smll.200400049
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The synthesis of 'Bamboo-like' and straight carbon nanotubes using thermolysis of Hexa-peri-hexabenzocoronene-cobalt complexes was analyzed. The compound was dissolved in dry dichloromethane and then Co[2(CO 8] was added. The thermolysis was carried in a sealed quartz tube with the temperature being controlled by an electronmagnetic oven. SEM measurements were performed on a LEO 1530 field emission scanning electron microscope. Results show that the obtained catrbon nanostructures depend on the3 heating process employed. Similar metal-polycyclic aromatic hydrocarbon complexxes will be synthesized and thermolyzed to further understand the role of graphitic PAHs in the precursor complexes.
引用
收藏
页码:210 / 212
页数:3
相关论文
共 50 条
  • [31] Cobalt particles encapsulated and nitrogen-doped bamboo-like carbon nanotubes as a catalytic and adsorptive bifunctional material for efficient removal of organic pollutants from wastewater
    Chen, Mantang
    Zhu, Lihua
    Zhang, Yuan
    Zou, Jing
    Tang, Heqing
    JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING, 2017, 5 (06): : 5322 - 5330
  • [32] SOLID-STATE MECHANOCHEMICAL SYNTHESIS OF COBALT(III), IRON(III), AND CHROMIUM(III) BISDICARBOLLYL COMPLEXES
    BORISOV, AP
    MAKHAEV, VD
    USYATINSKII, AY
    BREGADZE, VI
    RUSSIAN CHEMICAL BULLETIN, 1993, 42 (10) : 1637 - 1639
  • [33] One-pot chemical blasting synthesis of the bamboo-like multiwalled carbon nanotubes/graphene oxide nanocomposite and its application in electrochemical detection of dopamine
    Hongyu Yang
    Yunchun Li
    Yu Liu
    Yunsong Zhang
    Ying Zhao
    Maojun Zhao
    Journal of Solid State Electrochemistry, 2015, 19 : 145 - 152
  • [34] Synthesis, structure, solid-state thermolysis, and catalytic properties of binuclear Ce, Nd, Eu, and Gd cymantrenecarboxylate complexes with DMSO
    P. S. Koroteev
    Zh. V. Dobrokhotova
    A. B. Ilyukhin
    K. P. Birin
    M. S. Motornova
    V. M. Novotortsev
    Russian Chemical Bulletin, 2012, 61 : 1069 - 1078
  • [35] Synthesis, structure, solid-state thermolysis, and catalytic properties of binuclear Ce, Nd, Eu, and Gd cymantrenecarboxylate complexes with DMSO
    Koroteev, P. S.
    Dobrokhotova, Zh V.
    Ilyukhin, A. B.
    Birin, K. P.
    Motornova, M. S.
    Novotortsev, V. M.
    RUSSIAN CHEMICAL BULLETIN, 2012, 61 (06) : 1069 - 1078
  • [36] One-pot chemical blasting synthesis of the bamboo-like multiwalled carbon nanotubes/graphene oxide nanocomposite and its application in electrochemical detection of dopamine
    Yang, Hongyu
    Li, Yunchun
    Liu, Yu
    Zhang, Yunsong
    Zhao, Ying
    Zhao, Maojun
    JOURNAL OF SOLID STATE ELECTROCHEMISTRY, 2015, 19 (01) : 145 - 152
  • [37] Solid-State Synthesis of Polyaniline/Single-Walled Carbon Nanotubes: A Comparative Study with Polyaniline/Multi-Walled Carbon Nanotubes
    Abdiryim, Tursun
    Ubul, Aminam
    Jamal, Ruxangul
    Rahman, Adalet
    MATERIALS, 2012, 5 (07) : 1219 - 1231
  • [38] One-step solid-state synthesis of carbon nanotubes with surface functionality and their application in water treatment
    Yang, Shuangxia
    Wang, Lianying
    Yue, Shuang
    Guo, Xiaodi
    Song, Yufei
    He, Jing
    RSC ADVANCES, 2013, 3 (38): : 16990 - 16993
  • [39] Bamboo-like N,S-doped carbon nanotubes with encapsulated Co nanoparticles as high-performance electrocatalyst for liquid and flexible all-solid-state rechargeable Zn-air batteries
    Li, Zongnan
    Lin, Xiufang
    Xi, Wenhao
    Shen, Manrong
    Gao, Bifen
    Chen, Yilin
    Zheng, Yun
    Lin, Bizhou
    APPLIED SURFACE SCIENCE, 2022, 593
  • [40] Bamboo-like Composites of V2O5/Polyindole and Activated Carbon Cloth as Electrodes for All-Solid-State Flexible Asymmetric Supercapacitors
    Zhou, Xi
    Chen, Qiang
    Wang, Anqi
    Xu, Jian
    Wu, Shishan
    Shen, Jian
    ACS APPLIED MATERIALS & INTERFACES, 2016, 8 (06) : 3776 - 3783