3-{[3-(4-Methoxyphenyl)-4,5-dihydro-1,2-oxazol-5-yl]methyl}-1,5-dimethyl-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

被引：0

作者：

Dardouri, Rachida ^{[2
]}

Rodi, Yousef Kandri ^{[2
]}

Saffon, Natalie ^{[3
]}

Essassi, El Mokhtar ^{[4
]}

Ng, Seik Weng ^{[1
]}

机构：

[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia

[2] Univ Sidi Mohamed Ben Abdallah, Lab Chim Organ Appl, Fac Sci & Tech, Fes, Morocco

[3] Univ Toulouse 3, Serv Commun Rayons X FR2599, Toulouse, France

[4] Univ Mohammed V Agdal, Lab Chim Organ Herocycl, Rabat, Morocco

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

D O I：

10.1107/S1600536811022872

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The molecule of the title compound, C22H23N3O4, features a benzodiazepine fused-ring system whose seven-membered ring adopts a boat-shaped conformation (with the C atoms of the fused-ring as the stern and the methine C atom as the prow). The methylene C atom connected to the methine C atom occupies an equatorial position. The methylene C atom is connected to the five-membered oxazole ring, both of which are disordered over two positions in a 0.634 (4):0.366 (4) ratio. Weak intermolecular C-H center dot center dot center dot O hydrogen bonding is present in the crystal structure.

引用

页码：O1729 / U1054

页数：11

共 50 条

[21] Ultrasonic study of 5H-dibenz[B,F]azepine-5-carboxamide and 7-chloro-1,5-dihydro-1-methyl-5-phenyl-1,5-benzodiazepine-2,4(3H)-dione
Ravi, S.
Indira, S.
Natchimuthu, V.
Sengottaiyan, C.
INDIAN JOURNAL OF PURE & APPLIED PHYSICS, 2013, 51 (04) : 241 - 244
[22] 1-[3-(4-Chlorophenyl)-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-1-yl]-ethanone
Fun, Hoong-Kun
Quah, Ching Kheng
Samshuddin, S.
Narayana, B.
Sarojini, B. K.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1023 - +
[23] 4-[3-(Biphenyl-4-yl)-1-phenyl-4,5-dihydro-1H-pyrazol-5-yl]-3-(4-methoxyphenyl)-1-phenyl-1H-pyrazole dioxane monosolvate
Fun, Hoong-Kun
Arshad, Suhana
Malladi, Shridhar
Isloor, Arun M.
Shivananda, Kammasandra Nanjunda
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O972 - +
[24] 3-(4-Aminophenyl)-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazole-1-carbothioamide
Suwunwong, Thitipone
Chantrapromma, Suchada
Kumar, C. S. Chidan
Fun, Hoong-Kun
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1227 - +
[25] 1-[3-(4-methoxyphenyl)-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl]ethanone
Jian, Fang-Fang
Wang, Jing
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O5303 - O5304
[26] STRUCTURE OF 7-CHLORO-1-METHYL-5-PHENYL-1H-1,5-BENZODIAZEPINE-2,4(3H,5H)-DIONE (CLOBAZAM), C16H13CLN2O2
BUTCHER, HJ
HAMOR, TA
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1985, 41 (JUL) : 1081 - 1083
[27] 3-(4-Methoxybenzyl)-1,5-benzothiazepin- 4(5H)-one
Selvakumar, R.
Bakthadoss, M.
Vijayakumar, S.
Murugavel, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O693 - +
[28] Pelanserin: 3-[3-(4-phenylpiperazin-1-yl) propyl] quinazoline-2,4(1H,3H)-dione
Aguirre Hernandez, Gerardo
Somanathan, Ratnasamy
Bernes, Sylvain
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2014, 70 : O878 - +
[29] (E)-3-(4-Methoxyphenyl)-3-[3-(4-methoxyphenyl)-1H-pyrazol-1-yl] prop-2-enal
Susindran, V.
Athimoolam, S.
Bahadur, S. Asath
Manikannan, R.
Muthusubramanian, S.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O594 - +
[30] 6-[1-Acetyl-5-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazole-3-yl]-2(3H)-benzoxazolone
Ivanova, Yordanka
Todorova, Antonya
Chanev, Christo
Petrov, Ognyan
MOLBANK, 2018, (04)

← 1 2 3 4 5 →