Quantitative evaluation of the adhesion of metallic coatings using cylindrical substrate

This paper introduces an effective interfacial fracture toughness test based on interface fracture mechanics theory. This testing method uses a circumferentially notched tensile (CNT) specimen, which is ideally suited for determining the interfacial fracture resistance of coatings. Unlike other interfacial fracture tests, this test is simple to prepare, requires minimum test setup and is easy to model. An interfacial pre-crack was generated between a nickel coating and mild steel cylindrical substrate to evaluate adhesion strength. In situ acoustic and SEM analyses were used to determine the crack initiation or the critical load of failure. The critical energy release rate, critical stress intensity factors and phase angle were determined using the J integral which was determined by applying the critical load to the finite element model. A detailed finite element analysis was carried out to study the effect of different interface precrack positions and mode mixity on energy release rate for different notch angles and elastic modulus ratios. The cracking resistance of the interface was characterised by the notch angle of CNT specimens. The analysis showed an increase in interfacial fracture toughness as phase angle increases and was significant when the phase angle was large. The combined results of computational and experimental analysis showed that any defect or stress concentration at the interface could significantly weaken the adhesion of coating. (C) 2011 Elsevier Ltd. All rights reserved.