A variable temperature, ultrahigh vacuum atomic force microscope (AFM) was used to characterize interfacial friction for a single-asperity diamond contact on a diamondlike carbon (DLC) substrate over a nominal substrate temperature range of 90 to 275 K. Calibrated friction force measurements were obtained by analyzing lateral force hysteresis loops as a function of normal force. For sufficiently large normal forces, the lateral force was proportional to the normal force, and a friction coefficient mu could be identified. mu varied approximately linearly with substrate temperature, with mu=0.28 at T=90 K and mu=0.38 at 275 K. These results are compared to other recent variable temperature AFM friction measurements and to theoretical calculations based on the Tomlinson model. This comparison is obscured by large, experimentally uncontrolled temperature differences between the tip and the substrate which inevitably exist in conventional, variable temperature AFMs. A thermal model which can be used to quantitatively estimate these temperature differences is presented. (C) 2010 American Institute of Physics. [doi:10.1063/1.3436564]
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N Carolina State Univ, Dept Phys, Raleigh, NC 27695 USA
Arizona State Univ, Dept Phys, Tempe, AZ 85287 USAUSN Acad, Dept Chem, Annapolis, MD 21402 USA
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Univ Wisconsin, Mat Sci Program, Madison, WI 53706 USAUniv Wisconsin, Mat Sci Program, Madison, WI 53706 USA
Mishra, Maneesh
Egberts, Philip
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INM Leibniz Inst New Mat, D-66123 Saarbrucken, GermanyUniv Wisconsin, Mat Sci Program, Madison, WI 53706 USA
Egberts, Philip
Bennewitz, Roland
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INM Leibniz Inst New Mat, D-66123 Saarbrucken, GermanyUniv Wisconsin, Mat Sci Program, Madison, WI 53706 USA
Bennewitz, Roland
Szlufarska, Izabela
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Univ Wisconsin, Mat Sci Program, Madison, WI 53706 USA
Univ Wisconsin, Dept Mat Sci & Engn, Madison, WI 53706 USAUniv Wisconsin, Mat Sci Program, Madison, WI 53706 USA