Growth and characterization of a nonlinear optical crystal-2,6-diaminopyridinium 4-nitrophenolate 4-nitrophenol (DAPNP)

被引：47
|
作者：
Chen, Tianliang [1 ]
Sun, Zhihua [1 ]
Li, Lina [1 ]
Wang, Shuyun [1 ]
Wang, Yan [1 ]
Luo, Junhua [1 ]
Hong, Maochun [1 ]
机构：
[1] Chinese Acad Sci, Fujian Inst Res Struct Matter, Key Lab Optoelect Mat Chem & Phys, Fuzhou 350002, Fujian, Peoples R China
来源：
JOURNAL OF CRYSTAL GROWTH | 2012年 / 338卷 / 01期
关键词：
Solubility; Growth from solutions; Single crystal growth; Organic compounds; Nonlinear optic materials; 2ND-HARMONIC GENERATION; CRYSTAL; 2-AMINO-5-NITROPYRIDINIUM-TOLUENESULFONATE; BENZENESULFONIC ACIDS; DESIGN; SALT; HYPERPOLARIZABILITIES; COCRYSTALS; DIHYDRATE; RESPONSES; SHG;
D O I：
10.1016/j.jcrysgro.2011.10.023
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Bulk optical-quality single crystal of 2, 6-diaminopyridinium 4-nitrophenolate 4-nitrophenol (DAPNP) with dimensions of 22 x 15 x 8 mm(3) was successfully grown by the controlled slow cooling solution growth method. Thermogravimetric (TG) and differential thermal analysis (DTA) were carried out to characterize the thermal behaviors of the grown crystals. Its specific heat was determined and dielectric properties from 298.15 to 353.2 K have also been investigated. Second-harmonic generation (SHG) on powder samples indicated that DAPNP is a phase-matchable material and its SHG coefficient is 11.5 times larger than that of urea. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码：157 / 161
页数：5
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