NOVEL REGIOSELECTIVE SYNTHESIS OF 4-ISOTHIOCYANATOBUTAN-2-ONE BY A STAUDINGER REACTION. PREPARATION OF 6-UNSUBSTITUTED 4-HYDROXYHEXAHYDROPYRIMIDINE-2-THIONES

被引:1
|
作者
Dem'yachenko, E. A. [1 ]
Fesenko, A. A. [1 ]
Dobretsova, E. K. [1 ]
Fedorova, G. A. [1 ]
Shutalev, A. D. [1 ]
机构
[1] MV Lomonosov Moscow State Acad Fine Chem Technol, Moscow 119571, Russia
关键词
beta-azidocarbonyl compounds; 4-hydroxyhexahydropyrimidine-2-thiones; beta-isothiocyanato-carbonyl compounds; Staudinger reaction;
D O I
10.1007/s10593-010-0561-7
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
[No abstract available]
引用
收藏
页码:631 / 633
页数:3
相关论文
共 50 条
  • [1] Novel regioselective synthesis of 4-isothiocyanatobutan-2-one by a Staudinger reaction. preparation of 6-unsubstituted 4-hydroxyhexahydropyrimidine-2-thiones
    E. A. Demʼyachenko
    A. A. Fesenko
    E. K. Dobretsova
    G. A. Fedorova
    A. D. Shutalev
    Chemistry of Heterocyclic Compounds, 2010, 46 : 631 - 633
  • [2] Novel method for synthesis of 4-hydroxyhexahydropyrimidine-2-thiones
    1600, Springer Science and Business Media, LLC (31):
  • [3] NEW METHOD OF SYNTHESIS OF 4-HYDROXYHEXAHYDROPYRIMIDINE-2-THIONES
    SHUTALEV, AD
    KUKSA, VA
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1995, (01): : 97 - 102
  • [4] N-GLYCOSIDES .7. SYNTHESIS OF 4,5'-ANHYDRO-3-(2',3'-0-ISOPROPYLIDENE-BETA-D-RIBOFURANOSYL)-4-HYDROXYHEXAHYDROPYRIMIDINE-2-THIONES
    SHUTALEV, AD
    IGNATOVA, LA
    UNKOVSKII, BV
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1986, (12): : 1652 - 1657
  • [5] Synthesis of 4,6-Unsubstituted 2-Aminodihydropyrimidine-5-carboxylates through Sequential Staudinger/Aza-Wittig/Cyclization Reactions
    Nishimura, Yoshio
    Cho, Hidetsura
    SYNLETT, 2015, 26 (02) : 233 - 237
  • [6] Synthesis of 6-unsubstituted 2-oxo, 2-thioxo, and 2-amino-3, 4-dihydropyrimidines and their antiproliferative effect on HL-60 cells
    Nishimura, Yoshio
    Kikuchi, Hidetomo
    Kubo, Takanori
    Gokurakuji, Yuki
    Nakamura, Yuri
    Arai, Rie
    Yuan, Bo
    Sunaga, Katsuyoshi
    Cho, Hidetsura
    TETRAHEDRON LETTERS, 2020, 61 (28)
  • [7] Novel approach for the synthesis of N-unsubstituted 2,3,5,6-tetrahydro-4H-2,6-methano-1,3-benzoxazocine-4-thiones
    Alexander V. Borisov
    Svitlana S. Kovalenko
    Sergiy M. Kovalenko
    Chemistry of Heterocyclic Compounds, 2015, 51 : 678 - 681
  • [8] New Facilities of Biginelli Reaction. Synthesis of Methyl 6-Aryl-5-benzoyl-4-methoxy-2-oxohexahydropyrimidine-4-carboxylates
    Gein, V. L.
    Gorgopina, E. V.
    Zamaraeva, T. M.
    Dmitriev, M. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2017, 53 (11) : 1675 - 1677
  • [9] New facilities of Biginelli reaction. Synthesis of methyl 6-aryl-5-benzoyl-4-methoxy-2-oxohexahydropyrimidine-4-carboxylates
    V. L. Gein
    E. V. Gorgopina
    T. M. Zamaraeva
    M. V. Dmitriev
    Russian Journal of Organic Chemistry, 2017, 53 : 1675 - 1677
  • [10] Novel approach for the synthesis of N-unsubstituted 2,3,5,6-tetrahydro-4H-2,6-methano-1,3-benzoxazocine-4-thiones
    Borisov, Alexander V.
    Kovalenko, Svitlana S.
    Kovalenko, Sergiy M.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2015, 51 (07) : 678 - 681