Scanning transmission electron microscopy (STEM)-transmission electron microscopy (TEM) analysis of nitrogen ion implanted austenitic 302 stainless steel

被引:0
|
作者
Aggarwal, S [1 ]
Goodhew, PJ [1 ]
Murray, RT [1 ]
机构
[1] Univ Liverpool, Dept Mat Sci & Engn, Liverpool L69 3GH, Merseyside, England
关键词
nitrogen; ion implantation; scanning transmission electron microscopy (STEM); transmission electron microscopy (TEM); glancing angle X-ray diffraction (GXRD);
D O I
10.1016/S0040-6090(03)01233-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The microstructure of nitrogen implanted AISI 302 austenitic stainless steel and the effect of long-term room temperature ageing on it have been studied. Samples were implanted in 1992 with 2.5 x 10(21) N-2(+) m(-2) at 130 keV The characteristics of the implanted layer and the depth profile have been investigated by scanning transmission electron microscope combined with energy dispersive X-ray spectrometry. Electron diffraction patterns recorded in the implanted layer using transmission electron microscopy confirm the formation of CrN along with the presence of Cr2N. The identification of phases by glancing angle X-ray diffraction also indicates the formation of Cr2N and nitrogen solid solutions. The effects of ageing on the microstructure are observed to be small. (C) 2003 Elsevier B.V. All rights reserved.
引用
收藏
页码:12 / 17
页数:6
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