Low Temperature Synthesis of Single Crystalline Iron Hydroxide and Oxide Nanorods in Aqueous Media

被引：12

作者：

Chaudhari, Nitin K. ^{[1
]}

Fang, Baizeng ^{[1
]}

Bae, Tae-Sung ^{[2
]}

Yu, Jong-Sung ^{[1
]}

机构：

[1] Korea Univ, Res Team BK21, Dept Adv Mat Chem, Jochiwon 339700, Chungnam, South Korea

[2] Korea Basic Sci Inst, Jeonju Ctr, Jeonju 561756, South Korea

来源：

JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2011年 / 11卷 / 05期

关键词：

Iron Hydroxide (beta-FeOOH); Magnetic; Caffeine; Iron Oxide; BETA-FEOOH AKAGANEITE; ALPHA-FE2O3; NANORODS; SIZE; NANOPARTICLES; HYDROLYSIS; MORPHOLOGY; NANOWIRES; NANOTUBES; CAFFEINE; SILVER;

D O I：

10.1166/jnn.2011.3687

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An easy aqueous 'one-pot' synthesis route for the fabrication of single crystalline uniform iron hydroxide (beta-FeOOH) nanorods at low temperature is reported. beta-FeOOH nanorods with diameters of 5-37 nm and lengths up to 45-185 nm were obtained by varying the reaction parameters. Addition of ethanol was found to be crucial to control the aspect ratio. After calcination at 250 degrees C for 2 h the as-obtained beta-FeOOH nanorods was converted to alpha-Fe2O3 nanorods. To the best of our knowledge, beta-FeOOH nanorods having diameter less than 6 nm is reported for the first time.

引用

下载

页码：4457 / 4462

页数：6

共 50 条

[41] Low temperature chemical reaction synthesis of single-crystalline Eu(OH)3 nanorods and their thermal conversion to Eu2O3 nanorods
Du, Ning
Zhang, Hui
Chen, Bingdi
Wu, Jianbo
Li, Dongsheng
Yang, Deren
NANOTECHNOLOGY, 2007, 18 (06)
[42] Room-temperature synthesis of single-crystalline Se nanorods with remarkable photocatalytic properties
Chiou, Yao-De
Hsu, Yung-Jung
APPLIED CATALYSIS B-ENVIRONMENTAL, 2011, 105 (1-2) : 211 - 219
[43] Low temperature synthesis of single crystal ZnO microflower composed of hexagonal nanorods
Amutha, R.
Lee, Gang-Juan
Repo, Eveliina
Sillanpaa, Mika
Wu, Jerry J.
MATERIALS LETTERS, 2013, 107 : 64 - 67
[44] Synthesis and Characterization of Rutile Nanocrystals Prepared in Aqueous Media at Low Temperature
Kong, Linggen
Karatchevtseva, Inna
Blackford, Mark
Chironi, Ilkay
Triani, Gerry
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2012, 95 (02) : 816 - 822
[45] Synthesis of iron oxide nanorods for enhanced magnetic hyperthermia
Nikitin, Aleksey
Khramtsov, Maxim
Garanina, Anastasiia
Mogilnikov, Pavel
Sviridenkova, Natalya
Shchetinin, Igor
Savchenko, Alexander
Abakumov, Maxim
Majouga, Alexander
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2019, 469 : 443 - 449
[46] Synthesis of iron oxide nanoparticles under oxidizing environment and their stabilization in aqueous and non-aqueous media
Maity, D.
Agrawal, D. C.
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2007, 308 (01) : 46 - 55
[47] Hydrothermal synthesis of marcasite iron ditelluride FeTe2 nanorods at low temperature
Zhang, WX
Yang, ZH
Zhan, JH
Yang, L
Yu, WC
Zhou, GE
Qian, YT
MATERIALS LETTERS, 2001, 47 (06) : 367 - 370
[48] High-yield solvothermal synthesis of single-crystalline tin oxide tetragonal prism nanorods
Xia, Linsheng
Yang, Beifang
Fu, Zhengping
Yang, Yingling
Yan, Hongwei
Xu, Yuandong
Fu, Shengquan
Li, Gongpu
MATERIALS LETTERS, 2007, 61 (4-5) : 1214 - 1217
[49] Direct synthesis of highly crystalline single-phase hexagonal tungsten oxide nanorods by spray pyrolysis
Nakakura, Shuhei
Arif, Aditya Farhan
Rinaldi, Febrigia Ghana
Hirano, Tomoyuki
Tanabe, Eishi
Balgis, Ratna
Ogi, Takashi
ADVANCED POWDER TECHNOLOGY, 2019, 30 (01) : 6 - 12
[50] Large-Scale Synthesis of Single-Crystalline Iron Oxide Magnetic Nanorings
Jia, Chun-Jiang
Sun, Ling-Dong
Luo, Feng
Han, Xiao-Dong
Heyderman, Laura J.
Yan, Zheng-Guang
Yan, Chun-Hua
Zheng, Kun
Zhang, Ze
Takano, Mikio
Hayashi, Naoaki
Eltschka, Matthias
Klaeui, Mathias
Ruediger, Ulrich
Kasama, Takeshi
Cervera-Gontard, Lionel
Dunin-Borkowski, Rafal E.
Tzvetkov, George
Raabe, Joerg
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2008, 130 (50) : 16968 - 16977

← 1 2 3 4 5 →