Complete 1H and 13C NMR assignments of chamigrenes from Aplysia dactilomela

被引:16
|
作者
Kaiser, CR [1 ]
Pitombo, LF [1 ]
Pinto, AC [1 ]
机构
[1] Univ Fed Rio de Janeiro, Inst Quim, Ilha Fdn, CT, BR-21949900 Rio De Janeiro, Brazil
关键词
NMR; H-1; C-13; 2D NMR; Aplysia dactilomela; chamigrenes; johnstonol; pacifenediol; pacifidiene; pacifenol;
D O I
10.1002/mrc.800
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Stereochemical evaluation and complete H-1 and C-13 NMR assignment of the chamigrenes johnstonol (1), pacifenediol (2), pacifidiene (3), pacifenol (4), isolated from the Brazilian mollusc Aplysia dactilomela, were performed using 2D NMR techniques including COSY, NOESY, HSQC and HMBC, combined with AMI calculations and H-1 NMR spectrum simulations. Copyright (C) 2001 John Wiley & Sons, Ltd.
引用
收藏
页码:147 / 149
页数:3
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