Comparative investigation on antibacterial studies of Oxalis corniculata and silver nanoparticle stabilized graphene surface

被引:7
|
作者
Perumal, Suguna [1 ,2 ]
Atchudan, Raji [1 ]
Ramalingam, Srinivasan [3 ]
Edison, Thomas Nesakumar Jebakumar Immanuel [1 ]
Lee, Hyang Moo [4 ]
Cheong, In Woo [4 ]
Devarajan, Natarajan [5 ]
Lee, Yong Rok [1 ]
机构
[1] Yeungnam Univ, Sch Chem Engn, Gyongsan 38541, Gyeongsangbuk D, South Korea
[2] Sejong Univ, Dept Chem, Seoul 143747, South Korea
[3] Yeungnam Univ, Dept Food Sci & Technol, Gyongsan 38541, Gyeongsangbuk D, South Korea
[4] Kyungpook Natl Univ, Dept Appl Chem, Daegu 41566, South Korea
[5] Periyar Univ, Sch Biosci, Dept Biotechnol, Nat Drug Res Lab, Salem 636011, Tamil Nadu, India
基金
新加坡国家研究基金会;
关键词
ESCHERICHIA-COLI; GRAPHITE OXIDE; CHEMICAL-REDUCTION; BLOCK-COPOLYMERS; ESSENTIAL OILS; DISPERSIONS; MEMBRANE; EXFOLIATION; EXTRACTION; NANOSHEETS;
D O I
10.1007/s10853-022-07289-3
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, we report a facile method for the partial exfoliation of graphite into graphene and simultaneous surface stabilization of graphene and silver nanoparticles using a plant extract from Oxalis corniculata (Puliyarai Keerai). Four graphene composites were prepared through sonication: graphene-plant extract prepared at room temperature of about 27 degrees C (G-PRT) and 70 degrees C (G-PHT), and graphene-plant extract with silver nanoparticles prepared using NH4OH (G-PAgNH4) and NaOH (G-PAgNa). The composites were characterized using X-ray diffraction, Raman spectroscopy, field-emission scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and thermogravimetric analyses. The characterizations revealed the small sizes of the graphene sheets in the composites than in graphite, silver nanoparticles (AgNPs) with diameters of similar to 10 nm, and uniform distributions of the plant extract and AgNPs on the graphene surface. The graphene composites exhibited significant antibacterial potential against both Gram-negative (Salmonella typhimurium and Escherichia coli) and Gram-positive (Bacillus cereus and Staphylococcus aureus) microorganisms. G-PAgNa composites exhibited the lowest (10 mu g/mL) minimum inhibitory concentration and minimum bacterial concentration values against S. aureus and S. typhimurium. [GRAPHICS] .
引用
收藏
页码:11630 / 11648
页数:19
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