High-field 17O NMR studies of the SiOAl bond in solids

被引：73
|
作者：
Pingel, UT
Amoureux, JP
Anupold, T
Bauer, F
Ernst, H
Fernandez, C
Freude, D
Samoson, A
机构：
[1] Univ Leipzig, D-04103 Leipzig, Germany
[2] Univ Sci & Tech Lille Flandres Artois, F-59655 Villeneuve Dascq, France
[3] Estonian Acad Sci, Inst Chem Phys & Biophys, Tallinn, Estonia
来源：
CHEMICAL PHYSICS LETTERS | 1998年 / 294卷 / 4-5期
关键词：
D O I：
10.1016/S0009-2614(98)00847-1
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Oxygen-17 multiple-quantum magic-angle spinning and double rotation nuclear magnetic resonance studies were performed in the field of 17.6 T. A correlation between the isotropic value of the chemical shift and the SiOAl bond angle in zeolites was found. The correlation may be used for the determination of bond angles in SiOAl sites without long-range order. It is shown that multiple-quantum and double rotation techniques are complementary tools for getting highly-resolved O-17 NMR Spectra of solids. (C) 1998 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：345 / 350
页数：6
相关论文
共 50 条
  • [41] 17O NMR Studies of Yeast Ubiquitin in Aqueous Solution and in the Solid State
    Lin, Binyang
    Hung, Ivan
    Gan, Zhehong
    Chien, Po-Hsiu
    Spencer, Holly L.
    Smith, Steven P.
    Wu, Gang
    CHEMBIOCHEM, 2021, 22 (05) : 826 - 829
  • [42] 95Mo and 17O NMR studies of aqueous molybdate solutions
    Maksimovskaya, Raisa I.
    Maksimov, Gennady M.
    INORGANIC CHEMISTRY, 2007, 46 (09) : 3688 - 3695
  • [43] In vitro and in vivo studies of 17O NMR sensitivity at 9.4 and 16.4 T
    Lu, Ming
    Zhang, Yi
    Ugurbil, Kamil
    Chen, Wei
    Zhu, Xiao-Hong
    MAGNETIC RESONANCE IN MEDICINE, 2013, 69 (06) : 1523 - 1527
  • [44] 17O NMR studies on (E)-3-arylidenechromanone and -flavanones derivatives
    Tóth, G
    Simon, A
    Lévai, A
    Kählig, H
    Kalchhauser, H
    MAGNETIC RESONANCE IN CHEMISTRY, 2001, 39 (08) : 463 - 465
  • [45] High-field vortex dynamics in YB2Cu3O7 from 17O nuclear magnetic resonance
    Bachman, HN
    Reyes, AP
    Mitrovic, VF
    Halperin, WP
    Kleinhammes, A
    Kuhns, P
    Moulton, WG
    PHYSICAL REVIEW LETTERS, 1998, 80 (08) : 1726 - 1729
  • [46] HIGH-RESOLUTION O-17 NMR OF SOLIDS
    SCHRAMM, S
    OLDFIELD, E
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1984, 106 (09) : 2502 - 2506
  • [47] Synthesis and NMR studies of 17O enriched AM2O8 phases
    Hampson, MR
    Allen, S
    King, IJ
    Crossland, CJ
    Hodgkinson, P
    Harris, RK
    Fayon, F
    Evans, JSO
    SOLID STATE SCIENCES, 2005, 7 (07) : 819 - 826
  • [48] Endogenous Dynamic Nuclear Polarization for Natural Abundance 17O and Lithium NMR in the Bulk of Inorganic Solids
    Wolf, Tamar
    Kumar, Sandeep
    Singh, Harishchandra
    Chakrabarty, Tanmoy
    Aussenac, Fabien
    Frenkel, Anatoly I.
    Major, Dan Thomas
    Leskes, Michal
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2019, 141 (01) : 451 - 462
  • [49] ULTRA HIGH-FIELD NMR
    WEHRLI, FW
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1981, 181 (MAR): : 134 - ORGN
  • [50] Bond length-bond angle correlation in densified silica-Results from 17O NMR spectroscopy
    Trease, Nicole M.
    Clark, Ted M.
    Grandinetti, Philip J.
    Stebbins, Jonathan F.
    Sen, Sabyasachi
    JOURNAL OF CHEMICAL PHYSICS, 2017, 146 (18):
12345