Synthesis and crystal structure of 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-l-tosyl-1H-pyrrol-2(5H)-one

被引：0
|
作者：
Shen Ru-Wei [1 ]
Yang Yu-Zhu [1 ]
Cao Jian [1 ]
Wu Lu-Ling [1 ]
Huang Xian [1 ]
机构：
[1] Zhejiang Univ, Dept Chem, Hangzhou 310028, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2007年 / 26卷 / 12期
关键词：
4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one; synthesis; crystal structure;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The title compound 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-yl)-l-tosyl-IHpyrrol-2(5H)-one 1 (C24H22BrNO4S, M-r = 500.40) has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P2(1)/n with a = 8.8562(15), b = 18.118(3), c = 14.055(2) angstrom, beta = 99.855(3)degrees, V = 2221.9(6) angstrom(3), Z = 4, D, = 1.496 g/cm(3), p = 1.975 mm(-1), lambda = 0.71073 angstrom, F(000) 1024, R 0.0607 and wR = 0.1371.
引用
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页码：1505 / 1508
页数：4
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