Comparison of comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry and gas chromatography-mass spectrometry for the analysis of tobacco essential oils

被引：31
|
作者：
Zhu, SK
Lu, X
Xing, J
Zhang, SW
Kong, HW
Xu, GW
Wu, CY [1 ]
机构：
[1] Wuhan Univ, Dept Chem, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China
[2] Chinese Acad Sci, Dalian Inst Chem Phys, Natl Chromatogr R&A Ctr, Dalian 116011, Peoples R China
来源：
ANALYTICA CHIMICA ACTA | 2005年 / 545卷 / 02期
关键词：
gas chromatography-mass spectrometry; comprehensive two-dimensional gas chromatography; GC x GC; time-of-flight mass spectrometry; coupled columns; essential oil;
D O I：
10.1016/j.aca.2005.04.070
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A sample of tobacco essential oil was analyzed using gas chromatography-mass spectrometry (GUMS)and comprehensive two-dimensional gas chromatography coupled to a time-of-flight mass spectrometry (GC x GC/TOFMS), respectively. In the GUMS analysis, serially coupled columns were used. By comparing the GUMS results with GC x GC/TOFMS result,,, many more components in the essential oil could be found within the two-dimensional separation space of GC x GC. The quantitative determination of components in the essential oil was performed by GC x GC with flame ionization detection (FID), using a method of multiple internal standards calibration, (c) 2005 Elsevier B.V. All rights reserved.
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页码：224 / 231
页数：8
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