2-[(1S,3S)-3-Acetyl-2,2-dimethylcyclobutyl]-N-(2,6-difluorophenyl)acetamide

被引:4
|
作者
Yin, Yan-bai
Han, Chun-rui
Song, Zhan-qian [1 ]
Wang, Zong-de
机构
[1] Chinese Acad Forestry, Inst Chem Ind Forest Prod, Nanjing 210042, Peoples R China
[2] Jiangxi Agr Univ, Coll Forestry, Nanchang 330045, Peoples R China
关键词
D O I
10.1107/S1600536807043127
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C16H19F2NO2, was synthesized from 2,6-difluoro- benzenamine and 2-(3-acetyl-2,2-dimethyl-cyclo-butyl)-acetyl chloride, which was obtained through the reaction of 2-(3-acetyl-2,2-dimethyl-cyclo-butyl)acetic acid (pinonic acid) and thionyl chloride. The crystal structure involves N - H⋯O hydrogen bonds. © International Union of Crystallography 2007.
引用
收藏
页码:O4048 / U3033
页数:10
相关论文
共 50 条
  • [21] Study of Y(3S, 2S) → ηY(1S) and Y(3S, 2S) → π+ π- Y(1S) hadronic transitions
    Lees, J. P.
    Poireau, V.
    Tisserand, V.
    Garra Tico, J.
    Grauges, E.
    Martinelli, M.
    Milanes, D. A.
    Palano, A.
    Pappagallo, M.
    Eigen, G.
    Stugu, B.
    Brown, D. N.
    Kerth, L. T.
    Kolomensky, Yu. G.
    Lynch, G.
    Koch, H.
    Schroeder, T.
    Asgeirsson, D. J.
    Hearty, C.
    Mattison, T. S.
    McKenna, J. A.
    Khan, A.
    Blinov, V. E.
    Buzykaev, A. R.
    Druzhinin, V. P.
    Golubev, V. B.
    Kravchenko, E. A.
    Onuchin, A. P.
    Serednyakov, S. I.
    Skovpen, Yu. I.
    Solodov, E. P.
    Todyshev, K. Yu.
    Yushkov, A. N.
    Bondioli, M.
    Kirkby, D.
    Lankford, A. J.
    Mandelkern, M.
    Stoker, D. P.
    Atmacan, H.
    Gary, J. W.
    Liu, F.
    Long, O.
    Vitug, G. M.
    Campagnari, C.
    Hong, T. M.
    Kovalskyi, D.
    Richman, J. D.
    West, C. A.
    Eisner, A. M.
    Kroseberg, J.
    PHYSICAL REVIEW D, 2011, 84 (09):
  • [22] (S)-(-)-2-(1H-Indol-3-yl)-N-(1-phenylethyl) acetamide
    Ramirez, Johana
    Romero, Oscar
    Juarez, Jorge R.
    Teran, Joel L.
    Mendoza, Angel
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2252 - +
  • [23] Synthesis of (1R,cis)-2-(3-amino-2,2-dimethylcyclobutyl)ethanol, a precursor of cyclobutane carbocyclic nucleoside
    Borges, JER
    Fernandez, F
    Garcia, X
    Hergueta, AR
    Lopez, C
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1997, 29 (03) : 303 - 308
  • [24] Energy Calculation For Beryllium Atom in Different Excited States (1s2 2s 3s), (1s 2s2 3s) and (1s 2s 3s2)
    Al-Sharaa, Mayada J.
    Mahmood, Maysoon A.
    Madhkoor, Naaemh C. H.
    Al-Bayati, Khalil H.
    6TH INTERNATIONAL CONFERENCE AND WORKSHOPS ON BASIC AND APPLIES SCIENCES, 2017, 1888
  • [25] A third polymorph of 4-(2,6-difluorophenyl)-1,2,3,5-dithiadiazolyl
    Fatila, Elisabeth M.
    Jennings, Michael C.
    Goodreid, Jordan
    Preuss, Kathryn E.
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2010, 66 : O260 - O264
  • [26] N-(3,4-Difluorophenyl)-2,2-diphenylacetamide
    Fun, Hoong-Kun
    Ooi, Chin Wei
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1349 - +
  • [27] Magic wavelengths for the 2 3S → 2 1S transition in helium
    Notermans, R. P. M. J. W.
    Rengelink, R. J.
    van Leeuwen, K. A. H.
    Vassen, W.
    PHYSICAL REVIEW A, 2014, 90 (05):
  • [28] A Practical Synthesis of [(1S,3S)-3-Aminocyclohexyl]methanol and 2-[(1S,3S)-3-Aminocyclohexyl]propan-2-ol, Useful Intermediates for the Preparation of Novel mPGES-1 Inhibitors
    Walker, Daniel P.
    Heasley, Steven E.
    MacInnes, Allison
    Anjeh, Tizah
    Lu, Hwang-Fun
    Fobian, Yvette M.
    Collins, Joe T.
    Vazquez, Michael L.
    Mao, Michael K.
    SYNLETT, 2011, (20) : 2959 - 2962
  • [29] 1 IS, 2 1S AND 2 3S STATES OF H- AND OF HE
    PEKERIS, CL
    PHYSICAL REVIEW, 1962, 126 (04): : 1470 - &
  • [30] Luminescence Properties of 2-[2-Allyl(arenesulfonyl)oxyphenyl]-5-(2,6-difluorophenyl)-1,3,4-oxadiazoles
    Mikhailov, I. E.
    Artyushkina, Yu. M.
    Dushenko, G. A.
    Mikhailova, O. I.
    Revinskii, Yu. V.
    Minkin, V. I.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2018, 54 (12) : 1835 - 1838