Five-membered 2,3-dioxo heterocycles: LXXV. Reaction of methyl 1-aryl-3-aroyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates with 1,3-diphenylguanidine. Crystalline and molecular structure of 9-Benzoyl-8-hydroxy-2-imino-6-(4-methylphenyl)-1,3-diphenyl-1,3,6-triazaspiro-[4.4]non-8-ene-4,7-dione

被引：9

作者：

Bubnov, N. V. ^{[1
]}

Denislamova, E. S.

Aliev, Z. G. ^{[2
]}

Maslivets, A. N. ^{[1
]}

机构：

[1] Perm State Univ, Inst Nat Sci, Perm 614990, Russia

[2] Russian Acad Sci, Inst Chem Phys Problems, Chernogolovka 142432, Moscow Oblast, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2011年 / 47卷 / 04期

关键词：

SPIRO HETEROCYCLIZATION;

D O I：

10.1134/S1070428011040099

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Methyl 1-aryl-3-aroyl-4,5-dioxo-4,5-dihydro-1H-pyrrole-2-carboxylates reacted with 1,3-diphenylguanidine to give the corresponding 6-aryl-9-aroyl-8-hydroxy-2-imino-1,3-diphenyl-1,3,6-triazaspiro[4.4]non-8-ene-4,7-diones. The molecular and crystalline structures of 9-benzoyl-8-hydroxy-2-imino-6-(4-methylphenyl)-1,3-diphenyl-1,3,6-triazaspiro[4.4]non-8-ene-4,7-dione were determined by X-ray analysis.

引用

页码：523 / 526

页数：4

共 49 条

[31] Five-membered 2,3-dioxo heterocycles: LXIII. Cascade recyclization of isopropyl 2-(1-aryl-4,5-dioxo-2-phenyl-4,5-dihydro-1H-pyrrol-3-yl)-2-oxoacetates with cyclic enamines. Crystalline and molecular structure of 1′-benzyl-6′,6′-dimethyl-3-[(Z)-phenyl(phenylamino)methylidene]-6′,7′-dihydro-3H-spiro[furan-2,3′-indole]-2′,4,4′,5(1′H,5′H)-tetraone
P. S. Silaichev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 126 - 130
[32] Five-Membered 2,3-Dioxo Heterocycles: LXXI. Recyclization of 4,5-Diaroyl-1H-pyrrole-2,3-diones by the Action of Substituted Hydrazines. Crystalline and Molecular Structure of 2-(3-Benzoyl-1-benzyl-5-phenyl-1H-pyrazol-4-yl)-N-(4-methoxyphenyl)-2-oxoacetamide
Silaichev, P. S.
Kudrevatykh, N. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 46 (10) : 1546 - 1549
[33] Five-Membered 2,3-Dioxo Heterocycles: LXXI.* Recyclization of 4,5-Diaroyl-1H-pyrrole-2,3-diones by the Action of Substituted Hydrazines. Crystalline and Molecular Structure of 2-(3-Benzoyl- 1-benzyl-5-phenyl-1H-pyrazol-4-yl)-N-(4-methoxyphenyl)- 2-oxoacetamide
P. S. Silaichev
N. V. Kudrevatykh
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2010, 46 : 1546 - 1549
[34] Five-membered 2,3-dioxo heterocycles: XCI. Reaction of 3-aroyl-1H-pyrrolo[2,1-c][1,4]benzoxazine-1,2,4-triones with dimedone. Crystalline and molecular structure of 3′-benzoyl-4′-hydroxy-1′-(2-hydroxyphenyl)-6,6-dimethyl-6,7-dihydrospiro[1-benzofuran-3,2′-pyrrole]-2,4,5′(1′H,5H)-trione
Tutynina, N. M.
Racheva, N. L.
Maslivets, V. A.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2013, 49 (01) : 95 - 98
[35] Five-membered 2,3-dioxo heterocycles: XCI. Reaction of 3-aroyl-1H-pyrrolo[2,1-c][1,4]benzoxazine-1,2,4-triones with dimedone. Crystalline and molecular structure of 3′-benzoyl-4′-hydroxy-1′-(2-hydroxyphenyl)-6,6-dimethyl-6,7-dihydrospiro[1-benzofuran-3,2′-pyrrole]-2,4,5′(1′H,5H)-trione
N. M. Tutynina
N. L. Racheva
V. A. Maslivets
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2013, 49 : 95 - 98
[36] Five-membered 2,3-dioxo heterocycles: LXXVIII. Acylation of fischer's base with aroylketenes. Crystalline and molecular structure of (1E, 3Z)-4-(4-chlorophenyl)-4-hydroxy-1-(1,3,3-trimethyl-2,3-dihydro-1H-indol-2-ylidene)but-3-en-2-one
Konovalova, V. V.
Shklyaev, Yu. V.
Slepukhin, P. A.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2011, 47 (07) : 1062 - 1065
[37] Five-membered 2,3-dioxo heterocycles: LXXVIII. Acylation of fischer’s base with aroylketenes. Crystalline and molecular structure of (1E, 3Z)-4-(4-chlorophenyl)-4-hydroxy-1-(1,3,3-trimethyl-2,3-dihydro-1H-indol-2-ylidene)but-3-en-2-one
V. V. Konovalova
Yu. V. Shklyaev
P. A. Slepukhin
A. N. Maslivets
Russian Journal of Organic Chemistry, 2011, 47 : 1062 - 1065
[38] Five-membered 2,3-dioxo heterocycles: LXV. Reaction of 1-methyl-3,4-dihydroisoquinolines with aroylketenes. crystalline and molecular structure of (1Z,3Z)-4-hydroxy-1-[6,7-dimethoxy-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-4-phenylbut-3-en-2-one
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (10) : 1515 - 1518
[39] Five-membered 2,3-dioxo heterocycles: LXV. Reaction of 1-methyl-3,4-dihydroisoquinolines with aroylketenes. crystalline and molecular structure of (1Z,3Z)-4-hydroxy-1-[6,7-dimethoxy-3,3-dimethyl-3,4-dihydroisoquinolin-1(2H)-ylidene]-4-phenylbut-3-en-2-one
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 1515 - 1518
[40] Five-membered 2,3-dioxo heterocycles:: LXI.: Reaction of 3-aroyl-1H-pyrrolo[2,1-c][1,4]benzoxazine-1,2,4-triones with α-enamino esters.: Crystalline and molecular structure of methyl 11-benzoyl-2-o-hydroxyphenyl-3,4,10-trioxo-6,9-diphenyl-7-oxa-2,9-diazatricyclo[6.2.1.01,5]undec-5-ene-8-carboxylate
Racheva, N. L.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2008, 44 (08) : 1184 - 1188

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