Crystal Structure of 7-Phenyl-5,6-Dihydro-14-Aza-[1]benzopyrano[3,4-b]phenanthren-8H-One

被引：1

作者：

Sharma, Deepak ^{[1
]}

Sharma, Naresh ^{[2
]}

Patel, Niraj H. ^{[3
]}

Brahmbhatt, D., I ^{[4
]}

Gupta, Vivek K. ^{[5
]}

机构：

[1] Govt Girls Higher Secondary Sch, Miran Sahib, Jammu & Kashmir, India

[2] Govt Degree Coll Women, Kathua, Jammu & Kashmir, India

[3] Inst Sci & Technol Adv Studies & Res, Organ Chem Dept, Vallabh Vidyanagar, Gujarat, India

[4] Sarder Patel Univ, Dept Chem, Vallabh Vidyanagar, Gujarat, India

[5] Univ Jammu, Dept Phys, Jammu 180006, India

来源：

CRYSTALLOGRAPHY REPORTS | 2021年 / 66卷 / 07期

关键词：

Crystal structure;

D O I：

10.1134/S1063774521070142

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The crystal structure of the title compound is determined by single crystal X-ray structure analysis. The crystals are monoclinic, space group P2(1)/c, a = 13.607(3) angstrom, b = 13.352(3) angstrom, c = 9.700(2) angstrom, beta = 92.085(3)degrees, Z = 4, and R = 0.0543 for 3111 observed reflections. The dihedral angle between the coumarin nucleus and pyridine ring is 1.41(3)degrees, confirming the perfect planarity of the pyrido coumarin moiety. Ring D deviates significantly from planarity. The observed conformation for ring D is a half chair (Delta C-2(C5-C6) = 6.26). The supramolecular aggregation in the title compound is extremely simple and involves just one intermolecular hydrogen bond. Molecules are also reinforced by pi-pi stacking interactions involving pyrido coumarin moiety of the molecule.

引用

页码：1223 / 1226

页数：4

共 50 条

[31] SYNTHESIS OF LAMELLARINS VIA REGIOSELECTIVE ASSEMBLY OF 1,2-DIARYLATED [1]BENZOPYRANO[3,4-b]PYRROL-4(3H)-ONE CORE
Fukuda, Tsutomu
Katae, Takatoshi
Harada, Issei
Iwao, Masatomo
HETEROCYCLES, 2017, 95 (02) : 950 - 971
[32] Microwave assisted one pot synthesis of 8-methyl-3,6,9-triphenyl-5,6-dihydro-9H-pyrazolo [3,4-e] [1,2,4]triazolo[3,4-b][1,3,4]thiadiazepine
Nandeshwarappa, BP
Kumar, DBA
Naik, HSB
Vaidya, VP
Mahadevan, KM
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2005, 44 (10): : 2155 - 2157
[33] Pharmacological profile of 6,12-dihydro-3-methoxy-1-benzopyrano[3,4-b][1,4]benzothiazin-6-one, a novel human estrogen receptor agonist
Jacquot, Y
Cleeren, A
Laios, I
Ma, Y
Boulahdour, A
Bermont, L
Refouvelet, B
Adessi, G
Leclercq, G
Xicluna, A
BIOLOGICAL & PHARMACEUTICAL BULLETIN, 2002, 25 (03) : 335 - 341
[34] 1-ethyl-2-oxo-5-phenyl-1,6-dihydro-2H-oxazolo[4′,5′:5,6]pyrido[3,4-b]indole methanol hemisolvate
Yu, G
Li, YZ
Cao, LY
Zhang, XM
Wang, K
Hu, HW
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1271 - O1272
[35] CRYSTAL STRUCTURE OF 6-FERROCENYL-3-PHENYL-[1,2,4]TRIAZOLO[3,4-b][1,3,4] THIADIAZOLE
Wu, P.
JOURNAL OF STRUCTURAL CHEMISTRY, 2013, 54 (05) : 983 - 985
[36] Crystal structure of 6-ferrocenyl-3-phenyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
P. Wu
Journal of Structural Chemistry, 2013, 54 : 983 - 985
[37] SYNTHESIS OF 1-PHENYL-SUBSTITUTED 3-METHYL-1H-PYRAZOLO[3,4-B]PYRAZINE-5,6-DICARBOXYLIC ACID DIETHYL ESTERS
BARALDI, PG
SIMONI, D
PERIOTTO, V
MANFREDINI, S
GUARNERI, M
SYNTHESIS-STUTTGART, 1984, (02): : 148 - 149
[38] ANTIPARASITIC AGENTS .17. SYNTHESIS OF 2-METHYLMERCAPTO-7-H/PHENYL-1H,6H-PYRIDO[3,4-B]IMIDAZO[4,5-E]INDOLES, 6-(4-OXO-2-THIOQUINAZOLIN-3-YL]-1-H/PHENYL-9H-PYRIDO[3,4-B]INDOLES/8-(4-OXO-2-THIOQUINAZOLIN-3-YL)-1-H/PHENYL-9-H-PYRIDO[3,4-B]-INDOLES AND 6-(2,4-DIOXO-1,3-BENZOXAZIN-3-YL)-1-PHENYL-9H-PYRIDO[3,4-B]INDOLES/8-(2,4-DIOXO-1,3-BENZOXAZIN-3-YL)-1-PHENYL-9-H-PYRIDO[3,4-B]INDOLES AS ANTHELMINTIC AGENTS
AGARWAL, A
AGARWAL, SK
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1995, 34 (04): : 323 - 326
[39] 2-(3-Morpholinopropyl)-2,3-dihydro-1H-pyrrolo[3,4-b]quinolin-1-one monohydrate
Long, Yu-Hua
Zhou, Ting
Yang, Ding-Qiao
Wang, Wen-Ling
Zhang, Han-Mei
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O3180 - U737
[40] Crystal structure of (2-hydroxy-5-methylphenyl)(3-methyl-1-phenyl-1H-pyrazolo[3,4-b]pyridin-5-yl)methanone
Raja, Rajamani
Poomathi, Nataraj
Perumal, Paramasivam T.
SubbiahPandi, A.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O501 - U410

← 1 2 3 4 5 →