Facile synthesis of nanosized ε-Fe2O3 particles on the silica support

被引：43
|
作者：
Bukhtiyarova, G. A. [1 ]
Shuvaeva, M. A. [1 ]
Bayukov, O. A. [2 ]
Yakushkin, S. S. [1 ]
Martyanov, O. N. [1 ]
机构：
[1] Russian Acad Sci, Boreskov Inst Catalysis, Siberian Branch, Novosibirsk 630090, Russia
[2] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
来源：
JOURNAL OF NANOPARTICLE RESEARCH | 2011年 / 13卷 / 10期
关键词：
Supported nanoparticles; Heterogeneous catalysts; Synthesis; Magnetic nanoparticles; Electron spin resonance; OLEFIN CIS-DIHYDROXYLATION; MAGNETIC NANOPARTICLES; IRON; OXIDATION; HYDROGEN; CATALYSTS; GEL; DECOMPOSITION; OXYGEN; PHASE;
D O I：
10.1007/s11051-011-0542-5
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An approach is suggested to synthesize the epsilon-Fe2O3 particles supported on silica with the mean size of few nanometers, narrow size distribution and no admixture of any other iron oxide polymorphs. The facile synthesis is based on the pore filling impregnation method by iron sulfate (II) water solution with the following annealing procedure at similar to 1173 K. It is shown that the epsilon-Fe2O3 nanoparticles obtained are stable up to similar to 1173 K and possess superparamagnetic behavior up to similar to 870 K.
引用
收藏
页码：5527 / 5534
页数：8
相关论文
共 50 条
  • [21] Influence of Lithium on Nanosized Films of Fe2O3
    Turkovic, A.
    Ivanda, M.
    Bitenc, M.
    Orel, Z. Crnjak
    JOURNAL OF NANOMATERIALS, 2011, 2011
  • [22] Facile synthesis of nanoscaled α-Fe2O3, CuO and CuO/Fe2O3 hybrid oxides and their electrocatalytic and photocatalytic properties
    Pan, Lu
    Tang, Jing
    Wang, Fengwu
    CENTRAL EUROPEAN JOURNAL OF CHEMISTRY, 2013, 11 (05): : 763 - 773
  • [23] Facile synthesis of porous Fe2O3 nanorods and their photocatalytic properties
    Liu, Xiaosi
    Chen, Kaikai
    Shim, Jae-Jin
    Huang, Jiarui
    JOURNAL OF SAUDI CHEMICAL SOCIETY, 2015, 19 (05) : 479 - 484
  • [24] Facile Synthesis of α-Fe2O3 Nanostructured Films with Controlled Morphology
    Wei, Qing
    Li, Zhengcao
    Zhang, Zhengjun
    Zhou, Qin
    MATERIALS TRANSACTIONS, 2009, 50 (06) : 1351 - 1354
  • [25] Facile synthesis and magnetic properties of cross α-Fe2O3 nanorods
    Jia, Xiaohua
    Yang, Lin
    Song, Haojie
    Su, Yingtao
    MICRO & NANO LETTERS, 2011, 6 (09): : 806 - 808
  • [26] Formation of ε-Fe2O3 nanocrystals through segregation in mesoporous silica particles
    Mori, Kazumi
    Oaki, Yuya
    Suda, Masayuki
    Einaga, Yasuaki
    Imai, Hiroaki
    CHEMISTRY LETTERS, 2008, 37 (08) : 814 - 815
  • [27] Magnetic behavior of γ-Fe2O3 nanocrystals dispersed in colloidal silica particles
    Tartaj, P
    González-Carreño, T
    Serna, CJ
    JOURNAL OF PHYSICAL CHEMISTRY B, 2003, 107 (01): : 20 - 24
  • [28] Facile synthesis of high-magnetization γ-Fe2O3/alginate/silica microspheres for isolation of plasma DNA
    Liu, J. W.
    Zhang, Y.
    Chen, D.
    Yang, T.
    Chen, Z. P.
    Pan, S. Y.
    Gu, N.
    COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2009, 341 (1-3) : 33 - 39
  • [29] The synthesis of maghemite and hematite (γ-Fe2O3, α-Fe2O3) nanospheres
    Dar, M. A.
    Ansari, S. G.
    Wahab, R.
    Kim, Young-Soon
    Shin, Hyung-Shik
    PROGRESS IN POWDER METALLURGY, PTS 1 AND 2, 2007, 534-536 : 157 - +
  • [30] Synthesis and physical characterization of γ-Fe2O3 and (α+γ)-Fe2O3 nanoparticles
    P. Bhavani
    N. Ramamanohar Reddy
    I. Venkata Subba Reddy
    Journal of the Korean Physical Society, 2017, 70 : 150 - 154
12345