Synthesis of nanocrystalline Si particles from a solid-state reaction during a ball-milling process

被引：16
|
作者：
Araujo-Andrade, C [1 ]
Espinoza-Beltrán, FJ [1 ]
Jiménez-Sandoval, S [1 ]
González-Hernández, J [1 ]
机构：
[1] CINVESTAV, IPN, Unidad Queretaro, Programa Posgrado Mat, Queretaro 76230, Qro, Mexico
来源：
SCRIPTA MATERIALIA | 2003年 / 49卷 / 08期
关键词：
mechanical milling; Raman spectroscopy; X-ray diffraction; nanocrystalline materials;
D O I：
10.1016/S1359-6462(03)00429-9
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Silicon particles with nanometric size were synthesized by mechanical milling using a high-energy ball miller. The Si nanoparticles, observed using Raman spectroscopy, were formed according to a solid-phase reaction between amorphous SiO2 and Al powders. The crystalline size was determined by fitting the Raman spectrum with a phonon confinement model. (C) 2003 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.
引用
收藏
页码：773 / 778
页数：6
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