Synthesis of nanocrystalline Si particles from a solid-state reaction during a ball-milling process

被引：16

作者：

Araujo-Andrade, C ^{[1
]}

Espinoza-Beltrán, FJ ^{[1
]}

Jiménez-Sandoval, S ^{[1
]}

González-Hernández, J ^{[1
]}

机构：

[1] CINVESTAV, IPN, Unidad Queretaro, Programa Posgrado Mat, Queretaro 76230, Qro, Mexico

来源：

SCRIPTA MATERIALIA | 2003年 / 49卷 / 08期

关键词：

mechanical milling; Raman spectroscopy; X-ray diffraction; nanocrystalline materials;

D O I：

10.1016/S1359-6462(03)00429-9

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Silicon particles with nanometric size were synthesized by mechanical milling using a high-energy ball miller. The Si nanoparticles, observed using Raman spectroscopy, were formed according to a solid-phase reaction between amorphous SiO2 and Al powders. The crystalline size was determined by fitting the Raman spectrum with a phonon confinement model. (C) 2003 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

引用

页码：773 / 778

页数：6

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