One-pot synthesis of ferrocenyl dithiocarbamates and their application in the detection of Cu2+

被引：1
|
作者：
Dong, Junyang [1 ,2 ]
Hu, Jianfeng [1 ,3 ]
Zhang, Hao [1 ,3 ]
机构：
[1] Inner Mongolia Univ, Coll Chem & Chem Engn, Hohhot 010021, Peoples R China
[2] Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Solid Lubricat, Lanzhou 730000, Peoples R China
[3] Inner Mongolia Key Lab Fine Organ Synth, Hohhot 010021, Peoples R China
来源：
NEW JOURNAL OF CHEMISTRY | 2022年 / 46卷 / 41期
基金：
中国国家自然科学基金;
关键词：
N-TOSYLHYDRAZONES; COUPLING REACTIONS; FLUORESCENT-PROBE; REAGENTS; STRAIGHTFORWARD; RECOGNITION; CHEMOSENSOR; EFFICIENT; ION;
D O I：
10.1039/d2nj04133b
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient method for the synthesis of ferrocenyl dithiocarbamate derivatives by means of simple condensation between dithiocarbamate and N-tosylhydrazone under green conditions is presented. This new synthetic method is metal-free, and has high yields and good functional group tolerance. Furthermore, compound 3e as a probe has shown excellent recognition of Cu2+ using optical and electrochemical methods. The detection limit for 3e-Cu2+ was 5.31 x 10(-7) M.
引用
收藏
页码：19834 / 19840
页数：7
相关论文
共 50 条
  • [1] One-pot synthesis of dithiocarbamates accelerated in water
    Azizi, N
    Aryanasab, F
    Torkiyan, L
    Ziyaei, A
    Saidi, MR
    [J]. JOURNAL OF ORGANIC CHEMISTRY, 2006, 71 (09): : 3634 - 3635
  • [2] An efficient one-pot synthesis of 2-hydroxyalkyl dithiocarbamates
    Cui, JL
    Ge, ZM
    Cheng, TM
    Li, RT
    [J]. SYNTHETIC COMMUNICATIONS, 2003, 33 (12) : 1969 - 1976
  • [3] Convenient one-pot synthesis of symmetrical dithiocarbamates
    Nami, SAA
    Siddiqi, KS
    [J]. SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, 2004, 34 (09): : 1581 - 1590
  • [4] A one-pot synthesis of alkyl ferrocenyl ketones
    Vukicevic, RD
    Vukicevic, M
    Ratkovic, Z
    Konstantinovic, S
    [J]. SYNLETT, 1998, (12) : 1329 - 1330
  • [5] One-pot synthesis of 2-ferrocenyl-substituted pyridines
    Karadeniz, Eda
    Zora, Metin
    [J]. TETRAHEDRON LETTERS, 2016, 57 (44) : 4930 - 4934
  • [6] One-Pot Convenient and High Yielding Synthesis of Dithiocarbamates
    Vinod K. Tiwari
    Archana Singh
    Hakkim A. Hussain
    Bhuwan B. Mishra
    Vyasji Tripathi
    [J]. Monatshefte für Chemie - Chemical Monthly, 2007, 138 : 653 - 658
  • [7] One-pot convenient and high yielding synthesis of dithiocarbamates
    Tiwari, Vinod K.
    Singh, Archana
    Hussain, Hakkim A.
    Mishra, Bhuwan B.
    Tripathi, Vyasji
    [J]. MONATSHEFTE FUR CHEMIE, 2007, 138 (07): : 653 - 658
  • [8] One-pot synthesis of copper nanocluster/Tb-MOF composites for the ratiometric fluorescence detection of Cu2+
    Liu, Piaotong
    Hao, Rusi
    Sun, Wenliang
    Lin, Ziyi
    Jing, Tianfeng
    [J]. LUMINESCENCE, 2022, 37 (10) : 1793 - 1799
  • [9] One-pot fabrication of polymer nanoparticle-based chemosensors for Cu2+ detection in aqueous media
    Zhang, Peisheng
    Chen, Jian
    Huang, Fuhua
    Zeng, Zhiqiang
    Hu, Jia
    Yi, Pinggui
    Zeng, Fang
    Wu, Shuizhu
    [J]. POLYMER CHEMISTRY, 2013, 4 (07) : 2325 - 2332
  • [10] One-Pot Synthesis of Cu2O Octahedron Particles and Their Catalytic Application
    Li, Biao
    Li, Dan
    Mu, Lei
    Yang, Sung Ik
    [J]. BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 2017, 38 (04): : 499 - 502
12345