DETERMINATION OF TRACE LEACHING PHTHALATE ESTERS IN WATER AND URINE FROM PLASTIC CONTAINERS BY SOLID-PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY-MASS SPECTROMETRY

被引：30

作者：

Lee, Maw-Rong ^{[1
]}

Lai, Feng-Ying ^{[1
]}

Dou, Jianpeng ^{[1
,2
]}

Lin, Keh-Liang ^{[3
]}

Chung, Li-Wen ^{[1
]}

机构：

[1] Natl Chung Hsing Univ, Dept Chem, Taichung 402, Taiwan

[2] Jilin Univ, Coll Biol & Agr Engn, Changchun 130023, Peoples R China

[3] Chung Shan Med Univ, Sch Med Lab & Biotechnol, Taichung, Taiwan

来源：

ANALYTICAL LETTERS | 2011年 / 44卷 / 04期

关键词：

Direct immersion solid-phase microextraction; Gas chromatography-mass spectrometry; Medical devices; Microwavable polypropylene container; Phthalate esters; Polyvinyl chloride; ENDOCRINE-DISRUPTING COMPOUNDS; ACID ESTERS; EXTRACTION; FIBER; WINE;

D O I：

10.1080/00032711003783077

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A sensitive method has been developed for determination of trace leaching phthalate esters (PAEs) in water and urine from plastic containers by direct immersion solid-phase micro-extraction (DI-SPME) coupled to gas chromatography-mass spectrometry (GC-MS). The limits of detection (LODs) for PAEs in water and urine had values between 0.2-8 ng L-1 and 4-70 ng L-1, respectively. The proposed method was successfully used for quantification of trace PAEs in water in microwavable polypropylene containers heated by microwave irradiation and in the urine of patients treated with a glucose injection using polyvinyl chloride tubing.

引用

页码：676 / 686

页数：11

共 50 条

[31] Development of a headspace solid-phase microextraction method combined with gas chromatography mass spectrometry for the determination of phthalate esters in cow milk
Feng, YL
Zhu, JP
Sensenstein, R
[J]. ANALYTICA CHIMICA ACTA, 2005, 538 (1-2) : 41 - 48
[32] Simultaneous determination of 15 BTEX hydroxyl biomarkers in urine by headspace solid-phase microextraction gas chromatography-mass spectrometry
Lee, Jeong-Eeh
Lim, Hyun-Hee
Shin, Ho-Sang
[J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2019, 174 : 115 - 122
[33] Rapid determination of benzyl chloride in water by nonequilibrium solid-phase microextraction-gas chromatography-mass spectrometry
Zhao, RS
Liu, RM
Cui, QX
[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2002, 30 (06) : 722 - 725
[34] Simple and automatic determination of aldehydes and acetone in water by headspace solid-phase microextraction and gas chromatography-mass spectrometry
Kim, Hyun-Ji
Shin, Ho-Sang
[J]. JOURNAL OF SEPARATION SCIENCE, 2011, 34 (06) : 693 - 699
[35] Miniaturized solid-phase microextraction coupled with gas chromatography-mass spectrometry for determination of endocrine disruptors in drinking water
Alimzhanova, Mereke
Mamedova, Madina
Ashimuly, Kazhybek
Alipuly, Alham
Adilbekov, Yerlan
[J]. FOOD CHEMISTRY-X, 2022, 14
[36] Solid-phase microextraction and gas chromatography-mass spectrometry for quantitative determination of chlordecone in water, plant and soil samples
Soler, Alain
Lebrun, Marc
Labrousse, Yoan
Wignier, Thierry
[J]. FRUITS, 2014, 69 (04) : 325 - 339
[37] Application of Single Drop Microextraction in the Determination of Phthalate Esters in Food by Gas Chromatography-Mass Spectrometry
Li Meigui
Li Yuanxing
Mao Liqiu
[J]. CHINESE JOURNAL OF CHROMATOGRAPHY, 2007, 25 (01) : 35 - 38
[38] Solid-phase microextraction gas chromatography-mass spectrometry determination of fragrance allergens in baby bathwater
J. Pablo Lamas
Lucia Sanchez-Prado
Carmen Garcia-Jares
Maria Llompart
[J]. Analytical and Bioanalytical Chemistry, 2009, 394 : 1399 - 1411
[39] Determination of triazines in soil leachates by solid-phase microextraction coupled to gas chromatography-mass spectrometry
Zambonin, CG
Palmisano, F
[J]. JOURNAL OF CHROMATOGRAPHY A, 2000, 874 (02) : 247 - 255
[40] Determination of diazepam in human plasma by solid-phase microextraction and capillary gas chromatography-mass spectrometry
De Oliveira, MH
Queiroz, MEC
Carvalho, D
Silva, SM
Lanças, FM
[J]. CHROMATOGRAPHIA, 2005, 62 (3-4) : 215 - 219

← 1 2 3 4 5 →