X-ray photoelectron spectroscopic studies of carbon-fiber surfaces .21. Comparison of carbon fibers electrochemically oxidized in acid using achromatic and monochromatic XPS

被引：0
|
作者：
Viswanathan, H [1 ]
Rooke, MA [1 ]
Sherwood, PMA [1 ]
机构：
[1] KANSAS STATE UNIV,DEPT CHEM,MANHATTAN,KS 66506
来源：
SURFACE AND INTERFACE ANALYSIS | 1997年 / 25卷 / 06期
关键词：
XPS; carbon fiber; achromatic; monochromatic; oxidize;
D O I：
10.1002/(SICI)1096-9918(199706)25:6<409::AID-SIA252>3.3.CO;2-H
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Amoco M40 PAN-based carbon fibers were electrochemically oxidized in a pilot plant system. The changes in the surface of the fibers were monitored using monochromatic x-ray photoelectron spectroscopy (XPS), A parallel experiment using achromatic x-radiation was conducted for comparison. Other graphitic materials were also studied, Decomposition of the fiber due to x-ray exposure could be effectively eliminated by using the monochromator, The use of monochromatic x-radiation produced considerable narrowing in the linewidth of the graphitic peak, This allowed the curve fitting of the component peaks to be performed with significantly greater confidence. (C) 1997 by John Whey & Sons, Ltd.
引用
收藏
页码：409 / 417
页数：9
相关论文
共 50 条
  • [41] EPR spectroscopic and X-Ray diffraction studies of carbon fibers with different mechanical properties
    A. L. Kovarskii
    V. V. Kasparov
    A. V. Krivandin
    O. V. Shatalova
    R. A. Korokhin
    A. M. Kuperman
    Russian Journal of Physical Chemistry B, 2017, 11 : 233 - 241
  • [42] EPR spectroscopic and X-Ray diffraction studies of carbon fibers with different mechanical properties
    Kovarskii, A. L.
    Kasparov, V. V.
    Krivandin, A. V.
    Shatalova, O. V.
    Korokhin, R. A.
    Kuperman, A. M.
    RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY B, 2017, 11 (02) : 233 - 241
  • [43] X-RAY PHOTOELECTRON SPECTROSCOPIC STUDIES OF CARBON-FIBERS .14. ELECTROCHEMICAL TREATMENT OF PITCH-BASED FIBERS AND THE SURFACE AND BULK STRUCTURE CHANGES MONITORED BY XPS, XRD, AND SEM
    XIE, YM
    SHERWOOD, PMA
    APPLIED SPECTROSCOPY, 1990, 44 (10) : 1621 - 1628
  • [44] X-RAY PHOTOELECTRON-SPECTROSCOPIC STUDIES OF CARBON-FIBRE SURFACES .5. THE EFFECT OF PH ON SURFACE OXIDATION
    KOZLOWSKI, C
    SHERWOOD, PMA
    JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS I, 1985, 81 : 2745 - 2756
  • [45] X-Ray Photoelectron Spectroscopic Studies of Carbon Fiber Surfaces. 10. Valence-Band Studies Interpreted by X-alpha Calculations and the Differences between Poly (acrylonitrile)- and Pitch-Based Fibers
    Xie, Yaoming
    Sherwood, Peter M. A.
    CHEMISTRY OF MATERIALS, 1989, 1 (04) : 427 - 432
  • [46] X-RAY PHOTOELECTRON SPECTROSCOPIC STUDIES OF CARBON-FIBERS .15. ELECTROCHEMICAL TREATMENT ON PITCH-BASED FIBERS BY POTENTIOSTATIC AND GALVANOSTATIC METHODS
    XIE, YM
    SHERWOOD, PMA
    APPLIED SPECTROSCOPY, 1991, 45 (07) : 1158 - 1165
  • [47] Porosity Content Evaluation in Carbon-Fiber/Epoxy Composites Using X-ray Computed Tomography
    Yang, Peng
    Elhajjar, Rani
    POLYMER-PLASTICS TECHNOLOGY AND ENGINEERING, 2014, 53 (03) : 217 - 222
  • [48] X-ray photoelectron spectroscopic studies of surface modified single-walled carbon nanotube material
    Lee, WH
    Kim, SJ
    Lee, WJ
    Lee, JG
    Haddon, RC
    Reucroft, PJ
    APPLIED SURFACE SCIENCE, 2001, 181 (1-2) : 121 - 127
  • [49] Characterisation of void and fiber distribution in 3D printed carbon-fiber/PEEK using X-ray computed tomography
    Sommacal, S.
    Matschinski, A.
    Drechsler, K.
    Compston, P.
    COMPOSITES PART A-APPLIED SCIENCE AND MANUFACTURING, 2021, 149
  • [50] Characterisation of void and fiber distribution in 3D printed carbon-fiber/PEEK using X-ray computed tomography
    Sommacal, S.
    Matschinski, A.
    Drechsler, K.
    Compston, P.
    Composites Part A: Applied Science and Manufacturing, 2021, 149
12345