Enthalpies of combustion and formation of fullerenes by micro-combustion calorimetry in a Calvet calorimeter

被引：12
|
作者：
Rojas-Aguilar, A [1 ]
Martínez-Herrera, M [1 ]
机构：
[1] IPN, Ctr Invest & Estudios Avanzados, Dept Quim, Mexico City, DF, Mexico
来源：
THERMOCHIMICA ACTA | 2005年 / 437卷 / 1-2期
关键词：
fullerene; micro-combustion calorimetry; heat flux calorimetry; enthalpy of combustion; enthalpy of formation;
D O I：
10.1016/j.tca.2005.06.029
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
A set of micro-combustion bombs has been adapted to a Setaram C80 Calvet calorimeter. The calorimetric constant of the micro-bomb in the measurement fluxmeter was determined by combustions with benzoic acid NIST 39j, giving an uncertainty of less than 0.03% for calibration. The experimental methodology of applying this micro-combustion device to the measurement of the energy of combustion of graphite, C-60 and C-70 is described. Accuracy of better than 0.08% is obtained in some cases. (C) 2005 Elsevier B.V All rights reserved.
引用
收藏
页码：126 / 133
页数：8
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