N-(5-Bromopyridin-2-yl)acetamide

被引：1
|
作者：
Fun, Hoong-Kun [1 ]
Shahani, Tara [1 ]
Kumar, Rajesha [2 ]
Isloor, Arun M. [2 ]
Shivananda, Kammasandra N. [3 ]
机构：
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia
[2] Natl Inst Technol Karnataka, Dept Chem, Mangalore 575025, India
[3] Technion Israel Inst Technol, Schulich Fac Chem, IL-32000 Haifa, Israel
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
data-to-parameter ratio = 25.5; mean σ(CC) = 0.003 Å; R factor = 0.031; single-crystal X-ray study; T = 296 K; wR factor = 0.081;
D O I：
10.1107/S1600536811027553
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title compound, C7H7BrN2O, contains two molecules, in one of which the methyl H atoms are disorderd over two orientations in a 0.57 (3):0.43 (3) ratio. The dihedral angles between the pyridine rings and the acetamide groups are 7.27 (11) and 8.46 (11)degrees. In the crystal, molecules are linked by N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds generating bifurcated R-2(1)(5) ring motifs, which in turn lead to [110] chains.
引用
收藏
页码：O2043 / U573
页数：10
相关论文
共 50 条
  • [21] 2-(4-Bromophenyl)-N-(pyrazin-2-yl)-acetamide
    Nayak, Prakash S.
    Narayana, B.
    Jasinski, Jerry P.
    Yathirajan, H. S.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O891 - +
  • [22] 2-(Naphthalen-1-yl)-N-(1,3-thiazol-2-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02464 - +
  • [23] Crystal structure and Hirshfeld surface analysis of N-(5-iodo-4-phenylthiazol-2-yl)acetamide
    Herrera-Espana, Angel D.
    Aguilera-Gonzalez, Jesus
    Mena-Rejon, Gonzalo J.
    Hernandez-Ortega, Simon
    Caceres-Castillo, David
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 717 - +
  • [24] N-(2,4-DIFORMYL-5-HYDROXYPHENYL)ACETAMIDE
    HOCKER, J
    GIESECKE, H
    ORGANIC SYNTHESES, 1981, 60 : 49 - 52
  • [25] N-[5-(1-naphthyl)pyrimidin-4-yl]acetamide oxime
    Okuda, Kensuke
    Watanabe, Hiromi
    Hirota, Takashi
    Ishida, Hiroyuki
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O195 - O196
  • [26] Crystal structures and Hirshfeld surface analyses of 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(pyridin-2-yl)acetamide and 2-[(4,6-diaminopyrimidin-2-yl)-sulfanyl]-N-(pyrazin-2-yl)acetamide
    Choudhury, Manisha
    Viswanathan, Vijayan
    Timiri, Ajay Kumar
    Sinha, Karij Nayan
    Jayaprakash, Venkatesan
    Velmurugan, Devadasan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 718 - +
  • [27] N-(2,6-Dichlorophenyl)-2-(naphthalen-1-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1385 - +
  • [28] N-(4-Chlorophenyl)-2-(naphthalen-1-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Nayak, Prakash S.
    Narayana, B.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02463 - +
  • [29] N-(4-Bromophenyl)-2-(naphthalen-1-yl)acetamide
    Fun, Hoong-Kun
    Quah, Ching Kheng
    Narayana, B.
    Nayak, Prakash S.
    Sarojini, B. K.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2926 - U415
  • [30] Vibrational, spectroscopic, molecular docking and density functional theory studies on N-(5-aminopyridin-2-yl)acetamide
    Asath, R. Mohamed
    Rekha, T. N.
    Premkumar, S.
    Mathavan, T.
    Benial, A. Milton Franklin
    JOURNAL OF MOLECULAR STRUCTURE, 2016, 1125 : 633 - 642
12345