Mono- and sym-pentahalogenated corannulenes: reaction optimization & purification by in process product analysis

被引：1
|
作者：
Xu, Bokai [1 ]
Guo, Tianjian [1 ]
Siegel, Jay [1 ]
机构：
[1] Tianjin Univ, Sch Pharmaceut Sci & Technol, 92 Weijin Rd, Tianjin 370001, Peoples R China
来源：
REACTION CHEMISTRY & ENGINEERING | 2022年 / 7卷 / 05期
基金：
美国国家科学基金会;
关键词：
DERIVATIVES;
D O I：
10.1039/d2re00010e
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A robust, mild & inexpensive synthetic route to mono-halogenated corannulene and a robust method for purifying and analyzing sym-pentachlorocorannulene from the ICl halogenation of corannulene is reported.
引用
收藏
页码：1230 / 1235
页数：6
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