pH Dependent structural diversity of lead compounds based on new flexible ligand [3-(2-pyridyl)-1-pyrazolyl] acetic acid

被引:19
|
作者
Li, Qiao-Yun [1 ]
He, Ming-Hua [1 ]
Shen, Zhen-Dong [1 ]
Yang, Gao-Wen [1 ]
Yuan, Zhi-Yong [1 ]
机构
[1] Changshu Inst Technol, Dept Chem & Mat Engn, Jiangsu Lab Adv Funct Mat, Changshu 215500, Jiangsu, Peoples R China
关键词
Pb(II); 3-(2-pyridyl)-1-pyrazolyl] acetic acid; Crystal structure; Luminescence; METAL-ORGANIC FRAMEWORK; COORDINATION POLYMERS; CRYSTAL-STRUCTURES; MAGNETIC-PROPERTIES; COMPLEXES; TEMPERATURE; MN; CO; CATALYSIS; CLUSTERS;
D O I
10.1016/j.inoche.2012.03.011
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Two new Pb(II)/pypza compounds, namely, [Pb-3(pypza)(2)Cl-4] (1) and [Pb(pypza)Cl](2) (Hpypza = [3-(2-pyridyl)-1-pyrazolyl] acetic acid), have been synthesized through a hydrothermal method under different pH conditions, and characterized by single-crystal X-ray diffraction, element analysis, infrared spectra (IR). Compound 1 shows an unusual one-dimensional structure while compound 2 displays a novel two-dimensional network framework. Furthermore, the luminescence properties of 1 and 2 were investigated at room temperature in the solid state. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:214 / 218
页数:5
相关论文
共 40 条
  • [1] Four novel coordination compounds containing Hpypza ligand [Hpypza = [3-(2-pyridyl)-1-pyrazolyl] acetic acid]
    Yang, Jie
    Shen, Lei
    Yang, Gao-Wen
    Li, Qiao-Yun
    Zhu, Liu-Liu
    Shen, Wei
    Ji, Cheng
    Shen, Xiao-Feng
    INORGANICA CHIMICA ACTA, 2012, 392 : 25 - 29
  • [2] Synthesis and Characterization of SmIII and EuIII Coordination Compounds of 3-(2-Pyridyl)-1-pyrazolyl Acetic Acid
    Zou, Jian Hua
    Liu, Qiao
    Dong, Jia Fang
    Cao, Meng Jie
    Wu, Qian Qian
    Yue, Qiu Yan
    Li, Qiao Yun
    Yang, Gao Wen
    AUSTRALIAN JOURNAL OF CHEMISTRY, 2015, 68 (07) : 1152 - 1159
  • [3] Synthesis and characterizations of three layered ZnII, CdII and MnII coordination polymers with a flexible ligand [3-(2-pyridyl)-1-pyrazolyl] acetic acid
    Wang, Lei
    Jing, Guang-Peng
    Yang, Pei
    Chen, Jing
    JOURNAL OF COORDINATION CHEMISTRY, 2015, 68 (08) : 1295 - 1305
  • [4] Complexes of thallium(I) and lead(II) with the potentially tetradentate ligand bis[3-(2-pyridyl)-pyrazolyl]dihydroborate
    Bardwell, DA
    Jeffery, JC
    McCleverty, JA
    Ward, MD
    INORGANICA CHIMICA ACTA, 1998, 267 (02) : 323 - 328
  • [6] Crystal Structure and Spectroscopic Studies of a Dimeric Europium( III) ∼- Diketonate Complex Containing [ 3-( 2-Pyridyl)-1-pyrazolyl] acetate
    Coelho, Ana C.
    Gomes, Ana C.
    Fernandes, Jose A.
    Almeida Paz, Filipe A.
    Braga, Susana S.
    Rino, Luis
    Pereira, Luiz
    Pillinger, Martyn
    Goncalves, Isabel S.
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2014, 2014 (08) : 1284 - 1288
  • [7] Microwave assisted synthesis of molybdenum and tungsten tetracarbonyl complexes with a pyrazolylpyridine ligand.: Crystal structure of cis-[Mo(CO)4{ethyl[3-(2-pyridyl)-1-pyrazolyl]acetate}]
    Coelho, Ana C.
    Paz, Filipe A. Almeida
    Klinowski, Jacek
    Pillinger, Martyn
    Goncalves, Isabel S.
    MOLECULES, 2006, 11 (12) : 940 - 952
  • [8] Assembly of 1-D and decanuclear cage compounds from copper halide, cyclohexenephosphonic acid, and 3-(2-pyridyl) pyrazole
    Ma, Yun-sheng
    Yang, Zhen
    Cai, Wang-Shui
    Tang, Xiao-Yan
    Yuan, Rong-Xin
    JOURNAL OF COORDINATION CHEMISTRY, 2015, 68 (09) : 1633 - 1643
  • [9] A New Two-dimensional Cd(Ⅱ) Complex Assembled by 1,3,5-Benzenetricarboxylic Acid and 3-(2-Pyridyl)pyrazole
    王秀艳
    李秀梅
    潘亚茹
    刘博
    周实
    Chinese Journal of Structural Chemistry, 2019, 38 (08) : 1275 - 1282
  • [10] pH Dependent Synthesis of NdIII Coordination Compounds Based on Bifunctional 5-(4-Pyridyl)tetrazole-2-acetic Acid
    Cao, Meng Jie
    Li, Yue Kang
    Sun, Peng Peng
    Zhang, Chen Yi
    Wang, Jue
    Li, Qiao Yun
    Yang, Gao Wen
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2016, 642 (21): : 1218 - 1221