Solvent-free mechanochemical and liquid-phase reaction of [60]fullerene with ethyl 2-diazopropionate

被引：0
|
作者：
Li, YJ
Peng, RF
Liu, YC
Wang, GW [1 ]
机构：
[1] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2004年 / 15卷 / 11期
关键词：
60]fullerene; ethyl; 2-diazopropionate; methanofullerene; fulleroid;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The solvent-free mechanochemical reaction and the liquid-phase reaction of C-60 with ethyl 2-diazopropionate prepared in situ or preformed from alanine ethyl ester hydrochloride and sodium nitrite have been investigated. Methanofullerene 1 and fulleroids 2 and 3 from these reactions were obtained, meanwhile the pyrazoline intermediate was not observed. Fulleroids 2 and 3 can be converted to methanofullerene 1 in refluxing toluene.
引用
收藏
页码：1265 / 1268
页数：4
相关论文
共 50 条
  • [1] Solvent-free Mechanochemical and Liquid-phase Reaction of [60]Fullerene with Ethyl 2-Diazopropionate
    Yu Jin LI1
    ChineseChemicalLetters, 2004, (11) : 1265 - 1268
  • [2] Solvent-Free Mechanochemical Reaction of [60]Fullerene with Phenylhydrazine Hydrochlorides
    Chen, Zhong-Xiu
    Zhu, Bo
    Wang, Guan-Wu
    LETTERS IN ORGANIC CHEMISTRY, 2008, 5 (01) : 65 - 68
  • [3] Mechanochemical arylation and alkylation of fullerene C60 under the solvent-free conditions
    Tanaka, T
    Komatsu, K
    SYNTHETIC COMMUNICATIONS, 1999, 29 (24) : 4397 - 4402
  • [4] Solvent-Free Polymorphism Control in a Covalent Mechanochemical Reaction
    Cincic, Dominik
    Brekalo, Ivana
    Kaitner, Branko
    CRYSTAL GROWTH & DESIGN, 2012, 12 (01) : 44 - 48
  • [5] Solvent-free liquid-phase synthesis of polyhydroquinoline derivatives under microwave irradiation
    Zhang, Xiao-Lan
    Sheng, Shou-Ri
    Liu, Xian-Liang
    Liu, Xiao-Ling
    ARKIVOC, 2007, : 79 - 86
  • [6] Solvent-Free and Liquid-Phase Iodination of Thiophene Derivatives with Potassium Dichloroiodate Monohydrate
    Sereda, Grigoriy
    Sarkar, Akash Mamon
    Hussain, Anwar
    Zefirov, Nikolai
    SYNTHESIS-STUTTGART, 2020, 52 (07): : 1140 - 1146
  • [7] The mechanochemical Scholl reaction - a solvent-free and versatile graphitization tool
    Graetz, Sven
    Beyer, Doreen
    Tkachova, Valeriya
    Hellmann, Sarah
    Berger, Reinhard
    Feng, Xinliang
    Borchardt, Lars
    CHEMICAL COMMUNICATIONS, 2018, 54 (42) : 5307 - 5310
  • [8] The Reaction of Fullerene C60 with Phthalazine:: The Mechanochemical Solid-State Reaction Yielding a New C60 Dimer versus the Liquid-Phase Reaction Affording an Open-Cage Fullerene
    Murata, Y
    Kato, N
    Komatsu, K
    JOURNAL OF ORGANIC CHEMISTRY, 2001, 66 (22): : 7235 - 7239
  • [9] Mechanochemical reaction pathways in solvent-free synthesis of ZSM-5
    Nada, Majid H.
    Gillan, Edward G.
    Larsen, Sarah C.
    MICROPOROUS AND MESOPOROUS MATERIALS, 2019, 276 : 23 - 28
  • [10] Synthesis of Ni-based fluoroperovskites by solvent-free mechanochemical reaction
    Jin San Choi
    Muhammad Sheeraz
    Fazli Akram
    Hyoung-Su Han
    Jae-Shin Lee
    Chang Won Ahn
    Tae Heon Kim
    Journal of the Korean Physical Society, 2021, 79 : 1042 - 1050
12345