Colorimetric and Fluorescent Determination of Fluoride Using a Novel Naphthalene Diimide Boronic Acid Derivative
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作者:
Solis-Delgado, Luis Ernesto
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Inst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, MexicoInst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, Mexico
Solis-Delgado, Luis Ernesto
[1
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Ochoa-Teran, Adrian
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Inst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, MexicoInst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, Mexico
Ochoa-Teran, Adrian
[1
]
Yatsimirsky, Anatoly K.
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Univ Nacl Autonoma Mexico, Fac Quim, Mexico City, DF, MexicoInst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, Mexico
Yatsimirsky, Anatoly K.
[2
]
Pina-Luis, Georgina
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Inst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, MexicoInst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, Mexico
Pina-Luis, Georgina
[1
]
机构:
[1] Inst Tecnol Tijuana, Ctr Grad & Invest, Blvd Alberto Limon Padilla S-N,Campus Otay, Tijuana 22500, BC, Mexico
[2] Univ Nacl Autonoma Mexico, Fac Quim, Mexico City, DF, Mexico
A new 1,4,5,8-naphthalene diimide functionalized with two 3-phenylboronic acid groups (1) was prepared and used as a selective sensor for fluoride. The proposed sensor is based on anion-pi interactions between fluoride and naphthalene diimide core and the cooperative effect of boronic acid groups acting as Lewis acid anion receptors. The results show that the naphthalene diimide and boronic acid fragments participate in fluoride recognition. This modification significantly and positively affected the analytical response of the receptor. Interactions of 1 with fluoride were characterized by ultraviolet-visible, fluorescence, and nuclear magnetic resonance (NMR) spectroscopy. The influence of the boronic groups on the colorimetric and fluorescent properties was established by comparison with a non-functionalized aniline derivative. The sensor showed high selectivity in the presence of other anions. Colorimetric sensor 1 operated from 3.3 x 10(-4) to 1.5 x 10(-3) M with a detection limit of 3.6 x 10(-4) M. The fluorescent sensor operated from 0 to 4 x 10(-4) M allowing the measurement of 1.7 x 10(-5) M. The results open the possibility of design and development of a new class of naphthalene diimide receptors based on cooperative effects.
机构:
Ewha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
VL Coll Pharm, Dept Pharmaceut Chem, Raichur 584103, IndiaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Swamy, K. M. K.
Chung, So-Young
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Ewha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South KoreaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Chung, So-Young
Kim, Ha Na
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Ewha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South KoreaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Kim, Ha Na
Kim, Min Jung
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Ewha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South KoreaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Kim, Min Jung
Jeong, Yongsuk
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Ewha Womans Univ, Dept Bioinspired Sci, Seoul 120750, South KoreaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Jeong, Yongsuk
Yoon, Juyoung
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Ewha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
Ewha Womans Univ, Dept Bioinspired Sci, Seoul 120750, South KoreaEwha Womans Univ, Dept Chem & Nano Sci BK21, Seoul 120750, South Korea
机构:
Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Sun, Jingguo
Xu, Junhong
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North China Univ Water Resources & Elect Power, Dept Dynam Engn, Zhengzhou 450011, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Xu, Junhong
Ma, Qiujuan
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Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Ma, Qiujuan
Mao, Guojiang
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Henan Normal Univ, Henan Key Lab Organ Funct Mol & Drug Innovat, Collaborat Innovat Ctr Henan Prov Green Mfg Fine, Minist Educ Sch Chem & Chem Engn,Key Lab Green Ch, Xinxiang 453007, Henan, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Mao, Guojiang
Zhu, Nannan
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Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Zhu, Nannan
Tian, Meiju
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Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Tian, Meiju
Li, Linke
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Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
Li, Linke
Liu, Shuzhen
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Henan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R ChinaHenan Univ Chinese Med, Sch Pharm, Zhengzhou 450046, Peoples R China
机构:Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China
Huang, Jun-Chao
Li, De-Jia
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机构:Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China
Li, De-Jia
Diao, Jun-Chen
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机构:Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China
Diao, Jun-Chen
Hou, Jie
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机构:Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China
Hou, Jie
Yuan, Jiang-Lan
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机构:Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China
Yuan, Jiang-Lan
Zou, Guo-Lin
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Wuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R ChinaWuhan Univ, Coll Life Sci, State Key Lab Virol, Wuhan 430072, Peoples R China