Formation of self-organized Ta nano-structures by argon ion sputtering of Ta foil: XPS and AFM study

被引:30
|
作者
Medicherla, V. R. R. [1 ]
Majumder, S. [1 ]
Paramanik, D. [1 ]
Varma, Shikha [1 ]
机构
[1] Inst Phys, Bhubaneswar 751005, Orissa, India
关键词
Nano-structures; High dielectric oxides; Ion sputtering; XPS; Surface core level; AFM; Surface morphology; COMPOSITIONAL CHANGES; RIPPLE TOPOGRAPHY; THIN-FILMS; BOMBARDMENT; SURFACES; TA2O5; BEAM; TANTALUM; PARAMETERS; NANOSCALE;
D O I
10.1016/j.elspec.2010.02.006
中图分类号
O433 [光谱学];
学科分类号
0703 ; 070302 ;
摘要
The nano-structured Ta has been prepared by 3 keV argon ion sputtering of the Ta foil. The XPS and AFM studies were carried out on samples sputtered for fluences ranging from 6.0x10(15) to 3.6x10(16) ions/cm(2). The sample sputtered at lowest fluence showed the formation of dimples along with mild ripples which disappeared on further sputtering. After prolonged sputtering, clear ripple formation has been observed with a wave length of about 80 nm. Our XPS results indicated that Ta 4f of the Ta liberated after sputtering is shifted to higher binding energy by 0.5 eV. The Ta(2)O(5) completely disappeared after prolonged sputtering for 60 min, but little amount of sub-Ta oxide (TaO(x)) is still seen. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:1 / 5
页数:5
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