N-[3-(hydroxymethyl)phenyl]-N′-(4-methoxybenzoyl)thiourea

被引:0
|
作者
Ngah, N [1 ]
Fauzi, NFM [1 ]
Yamin, BM [1 ]
机构
[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Malaysia
关键词
D O I
10.1107/S1600536805007853
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The 4-methoxybenzoyl and 3-(hydroxymethyl) phenyl groups in the title compound, C16H16N2O3S, are trans and cis, respectively, with respect to the thione group across the C - N bonds. The central carbonylthiourea moiety makes dihedral angles with the 4-methoxybenzoyl and 3-( hydroxymethyl)phenyl fragments of 33.48 (7) and 45.96 (6) degrees, respectively. The molecules are stabilized by intermolecular N - H center dot center dot center dot O and O-H center dot center dot center dot S hydrogen bonds to form tetramers.
引用
收藏
页码:O1018 / O1019
页数:2
相关论文
共 50 条
  • [21] 1-[N-Methyl-N-(Phenyl)amino]-3-(4-Methylphenyl)Thiourea
    Yeo, Chien Ing
    Tiekink, Edward R. T.
    MOLBANK, 2019, (01)
  • [22] 2-Chloro-N-(4-methoxybenzoyl)benzene-sulfonamide
    Sreenivasa, S.
    Palakshamurthy, B. S.
    Pampa, K. J.
    Lokanath, N. K.
    Suchetan, P. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0199 - +
  • [23] N-(3-Methoxybenzoyl)-4- methyl-benzenesulfonamide
    Sreenivasa, S.
    Palakshamurthy, B. S.
    Lohith, T. N.
    Mohan, N. R.
    Kumar, Vijith
    Suchetan, P. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1263 - +
  • [24] Oxidation of N-(4-methoxybenzyl)-2-pyrrolidinones to N-(4-methoxybenzoyl)-2-pyrrolidinones. Rapid entry to optically active Aniracetam analogues.
    McAlonan, H
    Murphy, JP
    Stevenson, PJ
    Treacy, AB
    TETRAHEDRON, 1996, 52 (38) : 12521 - 12528
  • [25] N-(4-Chlorobenzoyl)-N′-(3-fluorophenyl)thiourea
    Othman, Nur Eliyanti A.
    Tahir, M. Ibrahim M.
    Yamin, Bohari M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2241 - U1703
  • [26] N-(3-methylphenyl)-N′-(4-nitrobenzoyl)-thiourea
    Xian, Liang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1969 - U4148
  • [27] 4-(4-METHOXYBENZOYL)-3-(2-METHYLALLYL)-TETRAHYDROPYRAN-2-ONE
    NIERLICH, M
    LANCE, M
    THUERY, P
    VIGNER, JD
    ROUX, MC
    WARTSKI, L
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1995, 51 : 673 - 674
  • [28] 2-[3-(4-Methoxybenzoyl)thioureido]-3-phenylpropionic acid methanol solvate
    Ngah, N
    Jusoh, A
    Yamin, BM
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O4307 - O4309
  • [29] 4-(4-Methoxybenzoyl)-3-(2-methylallyl)tetrahydropyran-2-one
    Nierlich, M.
    Lance, M.
    Thuery, P.
    Vigner, J.D.
    Roux, M.C.
    Wartski, L.
    Acta Crystallographica, Section C: Crystal Structure Communications, 1995, 51 (pt 4):
  • [30] N-(3-chloro-4-fluorophenyl)thiourea
    Rosli, Mohd Mustaqim
    Karthikeyan, Mari Sithambaram
    Fun, Hoong-Kun
    Razak, Ibrahim Abdul
    Patil, P. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O67 - O68