5-(2,4-dichlorobenzamido)-1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-1H-pyrazole-3-carbonitrile

被引：2
|
作者：
Zhong, P [1 ]
Zhang, XH [1 ]
Xiao, HP [1 ]
Hu, ML [1 ]
机构：
[1] Wenzhou Normal Coll, Dept Chem, Wenzhou 325027, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词：
D O I：
10.1107/S1600536805027054
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C18H7Cl4F3N4O, is a tricyclic amide with an overall U shape, each of the three rings being planar. The dihedral angle between the pyrazole and attached benzene ring is 90.1 (1)degrees. Intermolecular N-H center dot center dot center dot N hydrogen bonds, with an N(amide)center dot center dot center dot N(cyano) separation of 3.068 (6) angstrom, link the molecules.
引用
收藏
页码：O3110 / O3111
页数：2
相关论文
共 50 条
  • [21] 4-Bromo-5-[(4-chlorobenzylidene)-amino]-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-1H-pyrazole-3-carbonitrile
    Yu, Xiao-Chun
    Li, Shu-Yan
    Zhong, Ping
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3098 - U2531
  • [22] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-1H-pyrazole-3-carbonitrile
    Yang, ZP
    Zhong, P
    Hu, ML
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1351 - O1352
  • [23] 1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-iodo-4-trifluoromethylsulfinyl-1H-pyrazole-3-carbonitrile
    Jiang, Ding-Xin
    Xu, Han-Hong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1774 - U2229
  • [24] Crystal structure of 1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-5-((4-trifluoromethyl)methyleneimino)-1H-pyrazole-3-carbonitrile, C19H8Cl2F6N4
    Zhang, Xing-Guo
    Chen, Mu-Wang
    Hu, Mao-Lin
    Zhong, Ping
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (03): : 257 - 258
  • [25] 4-Bromo-1-[2,6-dichloro-4-(trifluoro-methyl)phenyl]-5-(4-nitrobenzylidene-amino)-1H-pyrazole-3-carbonitrile
    Yang, Zhiping
    Li, Shuyan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O645 - U1611
  • [26] 4-Bromo-1-[2,6-dichloro-4-(trifluoro-methyl)phenyl]-5-(4-methoxybenzyl-ideneamino)-1H-pyrazole-3-carbonitrile
    Zhu, Guohui
    Li, Shuyan
    Yang, Zhiping
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O646 - U1619
  • [27] Crystal structure of 1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-5-(4-bromobenzenesulfonylamide)-1H-pyrazole-3-carbonitrile, C17H8BrCl2F3N4O2S
    Zhang, Xiao-Hong
    Zhong, Ping
    Xiao, Hong-Ping
    Hu, Mao-Lin
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (01): : 69 - 70
  • [28] Crystal structure and mechanistic investigation of the reaction of 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-1H-pyrazole-3-carbonitrile with unsaturated carbonyl compounds
    Chuanxiang Liu
    Yong Chen
    Yingxin Sun
    Fanhong Wu
    Research on Chemical Intermediates, 2013, 39 : 2087 - 2093
  • [29] (E)-1-[2,6-dichloro-4-(trifluoromethyl)-phenyl]-5-[(dimethylamino)methyleneamino]-1H-pyrazole-4-carboxylic acid
    Xie, De-Ming
    Shu, Zhan
    Shen, Liang
    Ding, Zhe-Wu
    Jin, Zhi-Min
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4562 - U3701
  • [30] Crystal structure and mechanistic investigation of the reaction of 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-1H-pyrazole-3-carbonitrile with unsaturated carbonyl compounds
    Liu, Chuanxiang
    Chen, Yong
    Sun, Yingxin
    Wu, Fanhong
    RESEARCH ON CHEMICAL INTERMEDIATES, 2013, 39 (05) : 2087 - 2093
12345