9,9-Bis[4-(2-chloroethoxy)phenyl]-9H-fluorene

被引:0
|
作者
Shah, Kiramat [2 ]
Shah, Muhammad Raza [2 ]
Khan, Islam Ullah [3 ]
Ng, Seik Weng [1 ]
机构
[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia
[2] Univ Karachi, HEJ Res Inst Chem, Int Ctr Chem & Biol Sci, Karachi 75270, Pakistan
[3] Govt Coll Univ, Dept Chem, Lahore 54000, Pakistan
关键词
D O I
10.1107/S1600536810032046
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C(29)H(24)Cl(2)O(2), a fluorene derivative, features a C atom that is connected to four phenylene rings, two of which are almost coplanar (r.m.s. deviation = 0.035 angstrom) as they belong to the fluorene system. The other two rings are aligned at angles of 67.5 (5) and 85.5 (5)degrees with respect to the pair. The O and Cl atoms of the -OCH(2)CH(2)Cl- units adopt a gauche conformation [ torsion angles = 61.6 (6) and 66.6 (5)degrees].
引用
收藏
页码:O2317 / U389
页数:10
相关论文
共 50 条
  • [21] 2′,7′-Bis(4-methoxyphenyl)spiro[cyclopropane1,9′-9H-fluorene]
    Wang, ZX
    Lin, HY
    Lu, P
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O1084 - O1085
  • [22] Synthesis of 9,9-bis(4-hydroxyphenyl) fluorene catalyzed by bifunctional ionic liquids
    Wei, Jialun
    Yu, Limei
    Yan, Lei
    Bai, Wei
    Lu, Xinxin
    Gao, Zhanxian
    RSC ADVANCES, 2021, 11 (52) : 32559 - 32564
  • [23] Synthesis and characterisation of 9,9-bis(4-hydroxyphenyl)-fluorene catalysed by cation exchanger
    Liu, W.
    Wang, J.
    Qiu, Q. H.
    Ji, L.
    Wang, C. Y.
    Zhang, M. L.
    PIGMENT & RESIN TECHNOLOGY, 2008, 37 (01) : 9 - 15
  • [24] Novel fluorene-based biphenolic monomer: 9,9-bis(4-hydroxyphenyl)-9-silafluorene
    Seesukphronrarak, Surasak
    Takata, Toshikazu
    CHEMISTRY LETTERS, 2007, 36 (09) : 1138 - 1139
  • [25] AMIDINES DERIVATIVES OF 9H-FLUORENE
    FERRANTI, A
    CHIARINI, A
    GARUTI, L
    GIOVANNINETTI, G
    BRIGIDI, P
    FARMACO-EDIZIONE SCIENTIFICA, 1982, 37 (03): : 199 - 204
  • [26] 3,9'-Bi(9H-fluorene)
    Liu, Jie
    Yu, Wentao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2081 - +
  • [27] 2-[4-(tert-butylsulfanyl)benzyl]-9,9-diethyl-9H-fluorene
    Fan, Jian-Dong
    Yu, Wen-Tao
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : o1243 - o1244
  • [28] Synthesis of 9,9′-Bis(methoxymethyl)fluorene
    陈磊
    宋健
    冯荣秀
    吴小平
    Transactions of Tianjin University, 2003, (03) : 226 - 227
  • [29] The crystal structure of 1-(4-(2-chloroethoxy)phenyl)ethanone
    Li, Meng
    Bai, XueFeng
    Hou, YanJun
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2016, 231 (02): : 407 - 408
  • [30] Simple and clean synthesis of 9,9-bis[4-(2-hydroxyethoxy)phenyl]fluorene from the aromatic alkylation of phenoxyethanol with fluoren-9-one catalysed by titanium cation-exchanged montmorillonite
    Ebitani, K
    Kawabata, T
    Nagashima, K
    Mizugaki, T
    Kaneda, K
    GREEN CHEMISTRY, 2000, 2 (04) : 157 - 160