cis-1,2,3,6-tetrahydrophthalic anhydride at 173 K

被引：4
|
作者：
Bolte, M [1 ]
Bauch, C [1 ]
机构：
[1] Univ Frankfurt, Inst Organ Chem, D-60439 Frankfurt, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1999年 / 55卷
关键词：
D O I：
10.1107/S0108270198012402
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The title compound, C8H8O3, (I), crystallizes with two nearly identical molecules in the asymmetric unit. Each molecule has a boat conformation and noncrystallographic mirror symmetry. The structure was determined in connection with a study of the possible chemical decomposition of the compound in different solvents and in contact with the atmosphere. A similar boat conformation was found in five of six structures retrieved from the Cambridge Structural Database which contain (I) as a moiety. The present structure exhibits nearly the same packing motif as the recently found monoclinic polymorph.
引用
收藏
页码：226 / 228
页数：3
相关论文
共 50 条
  • [1] cis-1,2,3,6-Tetrahydrophthalic anhydride at 173 K
    Bolte, Michael
    Bauch, Christian
    Acta Crystallographica, Section C: Crystal Structure Communications, 1999, 55 (02): : 226 - 228
  • [2] cis-1,2,3,6-tetrahydrophthalic anhydride
    Ben Fredj, A
    Ben Redjeb, S
    Ben Amor, F
    Driss, A
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 1710 - 1712
  • [3] CONFORMATIONAL EQUILIBRIA IN CIS-1,2,3,6-TETRAHYDROPHTHALIC ANHYDRIDE SERIES
    LARTER, RM
    CRAIG, RER
    CRAIG, AC
    MUNDY, BP
    JOURNAL OF ORGANIC CHEMISTRY, 1977, 42 (07): : 1259 - 1261
  • [4] CONVERSION OF CIS-4-METHYL-1,2,3,6-TETRAHYDROPHTHALIC ANHYDRIDE ON METALLIC CATALYSTS
    DOKUCHAEVA, TG
    LEZDIN, SY
    LIBAROV, DA
    PADUTO, NV
    JOURNAL OF APPLIED CHEMISTRY OF THE USSR, 1985, 58 (09): : 1894 - 1900
  • [5] CONVERSION OF cis-4-METHYL-1,2,3,6-TETRAHYDROPHTHALIC ANHYDRIDE ON METALLIC CATALYSTS.
    Dokuchaeva, T.G.
    Lezdin, S.Yu.
    Libarov, D.A.
    Paduto, N.V.
    Journal of applied chemistry of the USSR, 1985, 58 (9 pt 2): : 1894 - 1900
  • [6] Mono- and bis-Quinidine Organocatalysts in the Asymmetric Methanolysis of Cis-1,2,3,6-Tetrahydrophthalic Anhydride: A Conformational and Mechanistic NMR Study
    Balzano, Federica
    Jumde, Ravindra P.
    Mandoli, Alessandro
    Masi, Sofia
    Pini, Dario
    Uccello-Barretta, Gloria
    CHIRALITY, 2011, 23 (09) : 784 - 795
  • [7] Potentiometric determination of maleic anhydride in the presence of cis-3,6-endomethylene-1,2,3,6-tetrahydrophthalic (endic) anhydride
    Yu. M. Evtushenko
    B. E. Zaitsev
    V. M. Ivanov
    Journal of Analytical Chemistry, 2000, 55 : 755 - 758
  • [8] Potentiometric determination of maleic anhydride in the presence of cis-3,6-endomethylene-1,2,3,6-tetrahydrophthalic (endic) anhydride
    Evtushenko, YM
    Zaitsev, BE
    Ivanov, VM
    JOURNAL OF ANALYTICAL CHEMISTRY, 2000, 55 (08) : 755 - 758
  • [9] Studies in iridoid synthesis.: Chemoselective transformations of cis-1,2,4,6-tetrahydrophthalic anhydride
    Stevens, Anne T.
    Bull, James R.
    Chibale, Kelly
    ORGANIC & BIOMOLECULAR CHEMISTRY, 2008, 6 (03) : 586 - 595
  • [10] IR SPECTROSCOPIC STUDY OF ESTERIFICATION OF CIS-3-METHYL-1,2,3,6-TETRAHYDROPHTHALIC ANHYDRIDE WITH NORMAL-BUTANOL
    YUKELSON, II
    ASHKOVA, VK
    EVSYUKOVA, TM
    KINETICS AND CATALYSIS, 1975, 16 (06) : 1225 - 1228
12345