Synthesis and characterization of a new double-cubane Mo-Fe-S cluster compound, [NEt(4)](3)[Mo2Fe6S8(mu-OMe)(3)(SPh)(3)Cl-3]

被引：5

作者：

Xu, JQ ^{[1
]}

Zhang, XG ^{[1
]}

Cai, H ^{[1
]}

Hu, NH ^{[1
]}

Wei, CP ^{[1
]}

Yang, GY ^{[1
]}

Wang, TG ^{[1
]}

机构：

[1] ACAD SINICA, CHANGCHUN INST APPL CHEM, CHANGCHUN 130022, JILIN, PEOPLES R CHINA

来源：

CHEMICAL COMMUNICATIONS | 1996年 / 06期

关键词：

D O I：

10.1039/cc9960000757

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The new double-cubane cluster compound [NEt(4)](3)[Mo2Fe6S8(mu-OMe)(3)(SPh)(3)Cl-3] is synthesized from (NH4)(2)MoS4, FeCl3, Fe powder, S powder, NaSPh and NEt(4)Br in MeOH-DMF, its crystal structure is determined by X-ray crystallography, and results of XPS indicate a valence state of +4 for Mo.

引用

页码：757 / 758

页数：2

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