Large scale hydrothermal synthesis of PbS nanorods

被引：36
|
作者：
Liang, Dadong [1 ]
Tang, Shanshan [2 ]
Liu, Jianbo [1 ]
Liu, Jinghua [1 ]
Lv, Xiaoli [1 ]
Kang, Lijuan [1 ]
机构：
[1] Jilin Agr Univ, Coll Resource & Environm Sci, Changchun 130118, Jilin, Peoples R China
[2] NE Normal Univ, Dept Chem, Changchun 130024, Jilin, Peoples R China
来源：
MATERIALS LETTERS | 2008年 / 62卷 / 15期
关键词：
PbS; semiconductors; nanomaterials; surfactant;
D O I：
10.1016/j.matlet.2007.12.012
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
PbS nanorods with a diameter of 20-50 nm have been synthesized successfully by surfactant-assisted hydrothermal route. The product was over 90% yield according to the amount of Pb(CH(3)CHOO)(2) used. Experiments showed that the concentration of N-cetyl-N,N,N-trimethyl-ammonium bromide (CTAB) and thiourea (Tu), reaction time and sulfur sources played important roles in the formation of the PbS nanorods. A reasonable mechanism for the formation of the PbS nanorods is also discussed. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码：2426 / 2429
页数：4
相关论文
共 50 条
  • [21] A Facile Green Synthesis of Ultranarrow PbS Nanorods
    Saah, Selina Ama
    Khan, Malik Dilshad
    Awudza, Johannes A. M.
    Revaprasadu, Neerish
    O'Brien, Paul
    [J]. JOURNAL OF INORGANIC AND ORGANOMETALLIC POLYMERS AND MATERIALS, 2019, 29 (06) : 2274 - 2281
  • [22] Sonochemical synthesis of PbS nanocubes, nanorods and nanotubes
    Wang, SF
    Gu, F
    Lü, MK
    Zhou, GJ
    Zhang, AY
    [J]. JOURNAL OF CRYSTAL GROWTH, 2006, 289 (02) : 621 - 625
  • [23] Hydrothermal synthesis of ZnO nanowires and nanobelts on a large scale
    Hu, Hanmei
    Huang, Xianhuai
    Deng, Chonghai
    Chen, Xiangying
    Qian, Yitai
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2007, 106 (01) : 58 - 62
  • [24] Facile synthesis of uniform tungsten oxide nanorods in large scale
    Zhang, B
    Cao, CB
    Qiu, HL
    Xu, YJ
    Wang, YC
    Zhu, HS
    [J]. CHEMISTRY LETTERS, 2005, 34 (02) : 154 - 155
  • [25] Synthesis of PbS microcrystals via a hydrothermal process
    Wang, SQ
    Pan, AL
    Yin, HY
    He, YP
    Lei, Y
    Xu, ZD
    Zou, BS
    [J]. MATERIALS LETTERS, 2006, 60 (9-10) : 1242 - 1246
  • [26] Hydrothermal synthesis and characterization of PbS nanorod bundles
    Zhu, Hua-Yun
    Zhang, Xiao-Bin
    Mi, Yu-Hong
    [J]. ACTA CHIMICA SINICA, 2008, 66 (03) : 398 - 402
  • [27] Facile large scale synthesis of WS2 nanotubes from WO3 nanorods prepared by a hydrothermal route
    Therese, HA
    Li, JX
    Kolb, U
    Tremel, W
    [J]. SOLID STATE SCIENCES, 2005, 7 (01) : 67 - 72
  • [28] Large-scale, surfactant-free, hydrothermal synthesis of lithium aluminate nanorods: Optimization of parameters and investigation of growth mechanism
    Joshi, Upendra A.
    Lee, Jae Sung
    [J]. INORGANIC CHEMISTRY, 2007, 46 (08) : 3176 - 3184
  • [29] Facile synthesis of PbS nanorods induced by concentration difference
    Sathyamoorthy, R.
    Kungumadevi, L.
    [J]. ADVANCED POWDER TECHNOLOGY, 2015, 26 (02) : 355 - 361
  • [30] Microwave Hydrothermal Synthesis of GaN Nanorods
    Li, Dong
    Wang, Fen
    Zhu, Jianfeng
    Liu, Dawei
    Wang, Xiaofeng
    Xiang, Liuyi
    [J]. ADVANCED MATERIAL SCIENCE AND TECHNOLOGY, PTS 1 AND 2, 2011, 675-677 : 251 - +
12345