Green Synthesis And Characterization of Ni0.8Zn0.2Fe2O4 Nano Ferrite

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作者
Raghuvanshi, S. [1 ]
Verma, R. [1 ]
Tiwari, P. [1 ,2 ]
Mazaleyrat, F.
Kane, S. N. [1 ,3 ]
机构
[1] DA Univ, Sch Phys, Magnet Mat Lab, Indore 452001, India
[2] Prestige Inst Engn Management & Res, Dept Phys, Indore 452010, India
[3] Univ Paris Saclay, SATIE, ENS Cachan, CNRS 8029, 61 Ave Pdt Wilson, F-94230 Cachan, France
来源
关键词
NANOPARTICLES;
D O I
10.1063/1.5122583
中图分类号
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号
07 ; 0710 ; 09 ;
摘要
Ni0.8Zn0.2Fe2O4 nano-powders were prepared by solution combustion method by using metal nitrates, citric acid, green fuel (plant extracts). The structural, magnetic characteristics of as prepared, annealed Ni0.8Zn0.2Fe2O4 samples were determined by X-ray diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR), vibrating sample magnetometer (VSM). XRD confirms the formation of single phase nano-crystalline (grain size: 12.7 - 32.7 nm) cubic spinel structure of annealed samples. Studied mixed ferrite shows relocation of Ni2+, Zn2+, Fe3+ ions between A, B site. Coercivity of annealed samples ranges between 29.7 to 124.9 Oe. Obtained saturation magnetization of annealed samples (34.56 - 54.96 Am-2/kg) is a combined effect of weakening of A-B, A-A, and strengthening of B-B interaction, and surface dead layer (0.80 - 1.25 nm) on particles, arising due to spin disorder at surface.
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页数:6
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