The synthesis and characterization of new metal-free and metallo phthalocyanines substituted with four dithiatetraoxa macrocyclic moieties

被引：2

作者：

Kantekin, Halit ^{[1
]}

Rakap, Murat

Misir, Mirac Nedim

Goek, Halil Zeki

Acar, Irfan

机构：

[1] Karadeniz Tech Univ, Dept Chem, TR-61080 Trabzon, Turkey

[2] Middle E Tech Univ, Dept Chem, TR-06531 Ankara, Turkey

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2007年 / 60卷 / 18期

关键词：

isoindolinediimine; nickel(II) phthalocyanine; mixed-donor macrocycle; template effect;

D O I：

10.1080/00958970701217412

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

New metal-free phthalocyanine ( 7) fused symmetrically in peripheral positions with four dithiatetraoxa macrocycles, has been synthesized by cyclotetramerization of the isoindoline-diimine derivative of macrocyclic 6. Metallophthalocyanine ( 8) was synthesized by reaction of phthalonitrile derivative ( 5) with anhydrous nickel( II) chloride. The new compounds were characterized by elemental analysis, H-1 and C-13-NMR, IR UV-Vis and mass spectroscopies.

引用

页码：1965 / 1972

页数：8

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