Microwave extraction of organochlorine pesticides from soils

被引：24
|
作者：
Concha-Graña, E [1 ]
Barriada-Pereira, M [1 ]
Turnes-Carou, MI [1 ]
Muniategui-Lorenzo, S [1 ]
López-Mahía, P [1 ]
Rodríguez, DP [1 ]
机构：
[1] Univ A Coruna, Dept Analyt Chem, La Coruna 15071, Spain
来源：
ANALYTICAL AND BIOANALYTICAL CHEMISTRY | 2003年 / 375卷 / 08期
关键词：
organochlorine pesticides; soil analysis; microwave-assisted extraction; pesticides; environmental analysis; GC-ECD;
D O I：
10.1007/s00216-003-1823-3
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
The purpose of this work was to develop a rapid, reliable and sensitive method for the extraction of organochlorine pesticides from soils using microwave energy with closed vessel technology. Three oven programs were assayed with two different solvent mixtures in order to achieve adequate experimental conditions for the complete extraction of organochlorine pesticides from the matrix. The method was validated using a certified reference soil material (CRM804-050).
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页码：1225 / 1228
页数：4
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