An efficient and greener approach to the synthesis of 3,5-dicyanopyridin-2 (1H)-one derivatives in aqueous media under microwave irradiation conditions

被引:8
|
作者
Jia, Runhong
Tu, Shujiang [1 ]
Zhang, Yan
Jiang, Bo
Zhang, Junyong
Yao, Changsheng
Shi, Feng
机构
[1] Lianyungang Teachers Coll, Jiangsu 222006, Peoples R China
[2] Xuzhou normal Univ, Coll Chem & Chem Engn, Xuzhou 221116, Peoples R China
关键词
D O I
10.1002/jhet.5570440533
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A facile and greener synthesis of a series of 3,5-dicyanopyridin-2(1H)-one derivatives was accomplished via the one-pot reaction of aldehyde, malononitrile and sodium hydroxide in aqueous media under microwave irradiation. This method had several advantages such as shorter route and time, lower cost, reduced environmental impact.
引用
收藏
页码:1177 / 1180
页数:4
相关论文
共 50 条
  • [21] Synthesis of 3,5-Bis(benzylidene)piperidin-4-one Derivatives in Water under Microwave Irradiation
    Peng, Juhua
    Han, Zhengguo
    Hao, Wenjuan
    Cao, Xudong
    Shi, Feng
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2009, 29 (08) : 1228 - 1231
  • [22] Synthesis and Optical Properties of Ethyl 2-Cyano-2-[3,4-dicyanopyridin-2(1H)-ylidene]acetate Derivatives
    S. S. Chunikhin
    O. V. Ershov
    Russian Journal of Organic Chemistry, 2021, 57 : 1103 - 1108
  • [23] Green and efficient synthesis of 2, 3-dihydroquinazolin-4(1H)-ones in aqueous medium using ZnFe2O4 catalyst under microwave irradiation
    Rupnar, Balaji D.
    Kachave, Tejswini R.
    Jawale, Pramod D.
    Shisodia, Suresh U.
    Pawar, Rajendra P.
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2017, 14 (09) : 1853 - 1858
  • [24] Green and efficient synthesis of 2, 3-dihydroquinazolin-4(1H)-ones in aqueous medium using ZnFe2O4 catalyst under microwave irradiation
    Balaji D. Rupnar
    Tejswini R. Kachave
    Pramod D. Jawale
    Suresh U. Shisodia
    Rajendra P. Pawar
    Journal of the Iranian Chemical Society, 2017, 14 : 1853 - 1858
  • [25] Synthesis and Optical Properties of Ethyl 2-Cyano-2-[3,4-dicyanopyridin-2(1H)-ylidene]acetate Derivatives
    Chunikhin, S. S.
    Ershov, O. V.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2021, 57 (07) : 1103 - 1108
  • [26] Novel approach to the synthesis of 3-amino-4-arylpyridin-2(1H)-one derivatives
    Shuvalov, Vladislav Yu.
    Chernenko, Sergei A.
    Shatsauskas, Anton L.
    Samsonenko, Anna L.
    Dmitriev, Maksim V.
    Fisyuk, Alexander S.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2021, 57 (7-8) : 764 - 771
  • [27] Novel Approach to the Synthesis of 3-amino-4-arylpyridin-2(1H)-one Derivatives
    Vladislav Yu. Shuvalov
    Sergei А. Chernenko
    Anton L. Shatsauskas
    Anna L. Samsonenko
    Maksim V. Dmitriev
    Alexander S. Fisyuk
    Chemistry of Heterocyclic Compounds, 2021, 57 : 764 - 771
  • [28] α-Zirconium Sulfophenylphosphonate as a Catalyst for the Synthesis of 3,4-Dihydropyrimidin-2(1H)-One Derivatives Under Solvent Free Conditions
    Rosati, Ornelio
    Curini, Massimo
    Montanari, Francesca
    Nocchetti, Morena
    Genovese, Salvatore
    CATALYSIS LETTERS, 2011, 141 (06) : 850 - 853
  • [29] α-Zirconium Sulfophenylphosphonate as a Catalyst for the Synthesis of 3,4-Dihydropyrimidin-2(1H)-One Derivatives Under Solvent Free Conditions
    Ornelio Rosati
    Massimo Curini
    Francesca Montanari
    Morena Nocchetti
    Salvatore Genovese
    Catalysis Letters, 2011, 141 : 850 - 853
  • [30] Synthesis of benzimidazole derivatives in an aqueous media and reflux conditions catalyzed by glycine at pH 5.2 under microwave approach
    Sasane, Nitin A.
    Valvi, Arun K.
    Meshram, Gangadhar S.
    Wadhawa, Gurumeet C.
    MATERIALS TODAY-PROCEEDINGS, 2022, 58 : 769 - 772