Catalytic synthesis of bis-2,3-dihydroquinazolin-4(1H)-ones and 2,3-dihydroquinazolin-4 (1H)-ones derivatives with the aid of silica-supported Preyssler nanoparticles (SPNP)

被引：0
|
作者：
Gharib, A. [1 ,2 ]
Vojdanifard, L. [3 ]
Pesyan, N. Noroozi [4 ]
Khorasani, B. R. Hashemi Pour [2 ]
Jahangir, M. [1 ]
Roshani, M. [1 ]
机构：
[1] Islamic Azad Univ, Dept Chem, Mashhad, Iran
[2] Agricultural Res & Serv Ctr, Mashhad, Iran
[3] Educ Org Razavi Khorasan, Educ Minist, Mashhad, Iran
[4] Urmia Univ, Fac Sci, Dept Chem, Orumiyeh 57159, Iran
来源：
BULGARIAN CHEMICAL COMMUNICATIONS | 2014年 / 46卷 / 04期
关键词：
Silica-supported Preyssler nanoparticles (SPNP); Heteropolyacid; 2,3-dihydroquinazolin-4(1H)-ones; Bisdihydroquinazolinones; Nanocatalyst; Isatoic anhydride; SOLID ACID CATALYST; 1,2-DIHYDROQUINAZOLIN-4(3H)-ONES; HETEROCYCLES; EFFICIENT;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
One-pot three-component condensation of isatoic anhydride with primary amines or ammonium carbonate and aromatic aldehydes in refluxing ethanol in the presence of catalytic amounts of silica-supported Preyssler nanoparticles (SPNP) afforded the corresponding 2,3-dihydroquinazolin-4(1H)-ones in high yields. Bis-dihydroquinazolinones were synthesized for the first time by a novel pseudo five-component condensation of isatoic anhydride, a primary amine, and a dialdehyde in water. The catalyst is reusable and can be applied several times without any decrease in product yield.
引用
收藏
页码：667 / 679
页数：13
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