ICP-MS determination of trace amounts of boron in high-purity quartz

被引：0
|
作者：
Karunasagar, D [1 ]
Dash, K [1 ]
Chandrasekaran, K [1 ]
Arunachalam, J [1 ]
机构：
[1] Natl Ctr Composit Characterizat Mat, Hyderabad 500062, Andhra Pradesh, India
来源：
ATOMIC SPECTROSCOPY | 2000年 / 21卷 / 06期
关键词：
D O I：
暂无
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
Boron at parts per billion levels was determined in high-purity quartz using an Inductively Coupled Plasma Mass Spectrometer (ICP-MS). The loss of boron due to volatilization during removal of the matrix was eliminated by adding mannitol. The recovery of boron was established by comparing the values obtained by external calibration with those obtained by isotope dilution. Recoveries of boron of similar to 95% were obtained when the mannitol-to-boron ratio was more than 10 (w/w). Using this method, the boron content of a number of high-purity quartz samples was determined.
引用
收藏
页码：216 / 219
页数：4
相关论文
共 50 条
  • [1] DETERMINATION OF TRACE AMOUNTS OF BORON IN HIGH-PURITY GRAPHITE BY ICP-MS
    MIYATANI, T
    SUZUKI, H
    YOSHIMOTO, O
    [J]. BUNSEKI KAGAKU, 1994, 43 (06) : 495 - 498
  • [2] ICP-MS determination of trace amounts of zinc, copper, lead and bismuth in high-purity aluminum after electrolytic separation
    Koyama, M
    Tanaka, T
    [J]. BUNSEKI KAGAKU, 2002, 51 (09) : 815 - 820
  • [3] Determination of trace elements in high-purity aluminum by solid-phase extraction/ICP-MS
    Hasegawa, S
    Yamaguchi, H
    Itoh, S
    Ide, K
    Kobayashi, T
    [J]. BUNSEKI KAGAKU, 2003, 52 (07) : 533 - 537
  • [4] Determination of trace elements in high-purity molybdenum by solid-phase extraction/ICP-MS
    Hasegawa, SI
    Yamaguchi, H
    Yamada, K
    Kobayashi, T
    [J]. MATERIALS TRANSACTIONS, 2004, 45 (03) : 925 - 929
  • [5] Determination of trace elements in high-purity molybdenum by solid-phase extraction/ICP-MS
    Hasegawa, S
    Yamaguchi, H
    Yamada, K
    Kobayashi, T
    [J]. JOURNAL OF THE JAPAN INSTITUTE OF METALS, 2005, 69 (01): : 127 - 131
  • [6] SPECTROPHOTOMETRIC DETERMINATION OF TRACE AMOUNTS OF BORON IN HIGH-PURITY GRAPHITE WITH CURCUMIN
    TOIDA, Y
    WATANABE, K
    [J]. BUNSEKI KAGAKU, 1993, 42 (05) : T65 - T69
  • [7] DETERMINATION OF TRACE AMOUNTS OF IMPURITIES IN HIGH-PURITY SILICON AND SILICATE MATERIALS BY VAPOR-PHASE PRESSURED DECOMPOSITION ICP-AES AND ICP-MS
    FUJIMOTO, K
    OKANO, T
    [J]. BUNSEKI KAGAKU, 1993, 42 (10) : T135 - T142
  • [8] Determining critical trace elements in high-purity hydrochloric acid by ICP-MS alone
    Jacksier, T
    Gluodenis, TJ
    Thomas, RJ
    [J]. MICRO, 1996, 14 (03): : 63 - &
  • [9] DETERMINATION OF TRACE AMOUNTS OF ZINC IN HIGH-PURITY ALUMINUM
    YOSHIMURA, W
    [J]. BUNSEKI KAGAKU, 1981, 30 (05) : 347 - 349
  • [10] Multichannel vapor phase digestion (MCVPD) of high purity quartz powder and the determination of trace impurities by ICP-AES and ICP-MS
    Dash, K
    Thangavel, S
    Dhavile, SM
    Chandrasekaran, K
    Chaurasia, SC
    [J]. ATOMIC SPECTROSCOPY, 2003, 24 (04) : 143 - 148
12345